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N,N′-[1,4-Phenylenebis(iminocarbonyl)]bis(l-phenylalanine) tetrahydrofuran disolvate
The title compound, C(26)H(26)N(4)O(6)·2C(4)H(8)O, representing a bis-urea with terminal phenylalanine units, crystallized with two tetrahydrofuran (THF) molecules. The main molecule is located on a crystallographic twofold axis, while the solvent molecule is disordered over two positions, wit...
Autores principales: | , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2023
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10561225/ https://www.ncbi.nlm.nih.gov/pubmed/37818468 http://dx.doi.org/10.1107/S2414314623007435 |
Sumario: | The title compound, C(26)H(26)N(4)O(6)·2C(4)H(8)O, representing a bis-urea with terminal phenylalanine units, crystallized with two tetrahydrofuran (THF) molecules. The main molecule is located on a crystallographic twofold axis, while the solvent molecule is disordered over two positions, with occupancies of 0.571 (15) and 0.429 (15). The host molecules are linked by N—H⋯O=C hydrogen bonds and C—H⋯O contacts with R (2) (1)(6) and R (2) (1)(7) ring motifs. The THF molecules enclosed in the crystal are connected to the bis-urea compound via O—H⋯O and C—H⋯O interactions. [Image: see text] |
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