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Bis(4-acetoxy-N-ethyl-N-n-propyltryptammonium) fumarate–fumaric acid (1/1)
The solid-state structure of the title salt/adduct (systemic name: bis{[2-(4-acetyloxy-1H-indol-3-yl)ethyl](ethyl)propylazanium} but-2-enedioate–(E)-butenedioic acid (1/1)), 2C(17)H(25)N(2)O(2) (+)·C(4)H(2)O(4) (2−)·C(4)H(4)O(4), was determined by single-crystal X-ray diffraction. The asymmetr...
| Autores principales: | , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2023
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10561228/ https://www.ncbi.nlm.nih.gov/pubmed/37818476 http://dx.doi.org/10.1107/S2414314623007794 |
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| author | Pham, Duyen N. K. Sackett, Nathan B. Chadeayne, Andrew R. Golen, James A. Manke, David R. |
| author_facet | Pham, Duyen N. K. Sackett, Nathan B. Chadeayne, Andrew R. Golen, James A. Manke, David R. |
| author_sort | Pham, Duyen N. K. |
| collection | PubMed |
| description | The solid-state structure of the title salt/adduct (systemic name: bis{[2-(4-acetyloxy-1H-indol-3-yl)ethyl](ethyl)propylazanium} but-2-enedioate–(E)-butenedioic acid (1/1)), 2C(17)H(25)N(2)O(2) (+)·C(4)H(2)O(4) (2−)·C(4)H(4)O(4), was determined by single-crystal X-ray diffraction. The asymmetric unit consists of a singly protonated tryptammonium cation, one half of a fumarate dianion and one half of a fumaric acid molecule. In the crystal, the ions and molecules are linked together in infinite chains propagating along [001] through a series of N—H⋯O and O—H⋯O hydrogen bonds. [Image: see text] |
| format | Online Article Text |
| id | pubmed-10561228 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2023 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-105612282023-10-10 Bis(4-acetoxy-N-ethyl-N-n-propyltryptammonium) fumarate–fumaric acid (1/1) Pham, Duyen N. K. Sackett, Nathan B. Chadeayne, Andrew R. Golen, James A. Manke, David R. IUCrdata Data Reports The solid-state structure of the title salt/adduct (systemic name: bis{[2-(4-acetyloxy-1H-indol-3-yl)ethyl](ethyl)propylazanium} but-2-enedioate–(E)-butenedioic acid (1/1)), 2C(17)H(25)N(2)O(2) (+)·C(4)H(2)O(4) (2−)·C(4)H(4)O(4), was determined by single-crystal X-ray diffraction. The asymmetric unit consists of a singly protonated tryptammonium cation, one half of a fumarate dianion and one half of a fumaric acid molecule. In the crystal, the ions and molecules are linked together in infinite chains propagating along [001] through a series of N—H⋯O and O—H⋯O hydrogen bonds. [Image: see text] International Union of Crystallography 2023-09-08 /pmc/articles/PMC10561228/ /pubmed/37818476 http://dx.doi.org/10.1107/S2414314623007794 Text en © Pham et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Data Reports Pham, Duyen N. K. Sackett, Nathan B. Chadeayne, Andrew R. Golen, James A. Manke, David R. Bis(4-acetoxy-N-ethyl-N-n-propyltryptammonium) fumarate–fumaric acid (1/1) |
| title | Bis(4-acetoxy-N-ethyl-N-n-propyltryptammonium) fumarate–fumaric acid (1/1) |
| title_full | Bis(4-acetoxy-N-ethyl-N-n-propyltryptammonium) fumarate–fumaric acid (1/1) |
| title_fullStr | Bis(4-acetoxy-N-ethyl-N-n-propyltryptammonium) fumarate–fumaric acid (1/1) |
| title_full_unstemmed | Bis(4-acetoxy-N-ethyl-N-n-propyltryptammonium) fumarate–fumaric acid (1/1) |
| title_short | Bis(4-acetoxy-N-ethyl-N-n-propyltryptammonium) fumarate–fumaric acid (1/1) |
| title_sort | bis(4-acetoxy-n-ethyl-n-n-propyltryptammonium) fumarate–fumaric acid (1/1) |
| topic | Data Reports |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10561228/ https://www.ncbi.nlm.nih.gov/pubmed/37818476 http://dx.doi.org/10.1107/S2414314623007794 |
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