4-Amino-3,5-di­chloro­pyridinium 3-hy­droxy­pico­linate monohydrate

In the title hydrated salt, C(5)H(5)Cl(2)N(2) (+)·C(6)H(4)NO(3) (−)·H(2)O, the pyridine N atom of the cation is protonated and an intra­molecular O—H⋯O hydrogen bond is observed in the anion, which generates an S(6) ring. The crystal packing features N—H⋯N, O—H⋯O, N—H⋯O, C—H⋯Cl and C—H⋯O hydrogen bo...

Descripción completa

Detalles Bibliográficos
Autores principales: Ashokan, Agalya, Nehru, Jayasudha, Chakkarapani, Nandhini, Khamrang, Themmila, Kavitha, Savaridasan Jose, Rajakannan, Venkatachalam, Hemamalini, Madhukar
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10561231/
https://www.ncbi.nlm.nih.gov/pubmed/37818469
http://dx.doi.org/10.1107/S2414314623008210
_version_ 1785117876650246144
author Ashokan, Agalya
Nehru, Jayasudha
Chakkarapani, Nandhini
Khamrang, Themmila
Kavitha, Savaridasan Jose
Rajakannan, Venkatachalam
Hemamalini, Madhukar
author_facet Ashokan, Agalya
Nehru, Jayasudha
Chakkarapani, Nandhini
Khamrang, Themmila
Kavitha, Savaridasan Jose
Rajakannan, Venkatachalam
Hemamalini, Madhukar
author_sort Ashokan, Agalya
collection PubMed
description In the title hydrated salt, C(5)H(5)Cl(2)N(2) (+)·C(6)H(4)NO(3) (−)·H(2)O, the pyridine N atom of the cation is protonated and an intra­molecular O—H⋯O hydrogen bond is observed in the anion, which generates an S(6) ring. The crystal packing features N—H⋯N, O—H⋯O, N—H⋯O, C—H⋯Cl and C—H⋯O hydrogen bonds, which generate a three-dimensional network. [Image: see text]
format Online
Article
Text
id pubmed-10561231
institution National Center for Biotechnology Information
language English
publishDate 2023
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-105612312023-10-10 4-Amino-3,5-di­chloro­pyridinium 3-hy­droxy­pico­linate monohydrate Ashokan, Agalya Nehru, Jayasudha Chakkarapani, Nandhini Khamrang, Themmila Kavitha, Savaridasan Jose Rajakannan, Venkatachalam Hemamalini, Madhukar IUCrdata Data Reports In the title hydrated salt, C(5)H(5)Cl(2)N(2) (+)·C(6)H(4)NO(3) (−)·H(2)O, the pyridine N atom of the cation is protonated and an intra­molecular O—H⋯O hydrogen bond is observed in the anion, which generates an S(6) ring. The crystal packing features N—H⋯N, O—H⋯O, N—H⋯O, C—H⋯Cl and C—H⋯O hydrogen bonds, which generate a three-dimensional network. [Image: see text] International Union of Crystallography 2023-09-22 /pmc/articles/PMC10561231/ /pubmed/37818469 http://dx.doi.org/10.1107/S2414314623008210 Text en © Ashokan et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Ashokan, Agalya
Nehru, Jayasudha
Chakkarapani, Nandhini
Khamrang, Themmila
Kavitha, Savaridasan Jose
Rajakannan, Venkatachalam
Hemamalini, Madhukar
4-Amino-3,5-di­chloro­pyridinium 3-hy­droxy­pico­linate monohydrate
title 4-Amino-3,5-di­chloro­pyridinium 3-hy­droxy­pico­linate monohydrate
title_full 4-Amino-3,5-di­chloro­pyridinium 3-hy­droxy­pico­linate monohydrate
title_fullStr 4-Amino-3,5-di­chloro­pyridinium 3-hy­droxy­pico­linate monohydrate
title_full_unstemmed 4-Amino-3,5-di­chloro­pyridinium 3-hy­droxy­pico­linate monohydrate
title_short 4-Amino-3,5-di­chloro­pyridinium 3-hy­droxy­pico­linate monohydrate
title_sort 4-amino-3,5-di­chloro­pyridinium 3-hy­droxy­pico­linate monohydrate
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10561231/
https://www.ncbi.nlm.nih.gov/pubmed/37818469
http://dx.doi.org/10.1107/S2414314623008210
work_keys_str_mv AT ashokanagalya 4amino35dichloropyridinium3hydroxypicolinatemonohydrate
AT nehrujayasudha 4amino35dichloropyridinium3hydroxypicolinatemonohydrate
AT chakkarapaninandhini 4amino35dichloropyridinium3hydroxypicolinatemonohydrate
AT khamrangthemmila 4amino35dichloropyridinium3hydroxypicolinatemonohydrate
AT kavithasavaridasanjose 4amino35dichloropyridinium3hydroxypicolinatemonohydrate
AT rajakannanvenkatachalam 4amino35dichloropyridinium3hydroxypicolinatemonohydrate
AT hemamalinimadhukar 4amino35dichloropyridinium3hydroxypicolinatemonohydrate

Ejemplares similares