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Synthesis and Investigation of Properties of Beryllium Ceramics Modified with Titanium Dioxide Nanoparticles

Samples of beryllium ceramics, with the addition of micro- and nanoparticles TiO(2,) have been obtained by the method of thermoplastic slip casting. The microstructure of batch ceramics, consisting of micropowders and ceramics with TiO(2) nanoparticles sintered at an elevated temperature, has been i...

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Autores principales: Pavlov, Alexandr, Sagdoldina, Zhuldyz, Zhilkashinova, Almira, Magazov, Nurtoleu, Turar, Zhangabay, Gert, Sergey
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10573473/
https://www.ncbi.nlm.nih.gov/pubmed/37834644
http://dx.doi.org/10.3390/ma16196507
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author Pavlov, Alexandr
Sagdoldina, Zhuldyz
Zhilkashinova, Almira
Magazov, Nurtoleu
Turar, Zhangabay
Gert, Sergey
author_facet Pavlov, Alexandr
Sagdoldina, Zhuldyz
Zhilkashinova, Almira
Magazov, Nurtoleu
Turar, Zhangabay
Gert, Sergey
author_sort Pavlov, Alexandr
collection PubMed
description Samples of beryllium ceramics, with the addition of micro- and nanoparticles TiO(2,) have been obtained by the method of thermoplastic slip casting. The microstructure of batch ceramics, consisting of micropowders and ceramics with TiO(2) nanoparticles sintered at an elevated temperature, has been investigated. It was found that the introduction of TiO(2) nanoparticles leads to changes in the mechanisms of mass transfer and microstructure formation, and the mobility of TiO(2) at interfacial grain boundaries increases, which leads to the formation of elements of a zonal shell structure. The reduction of intergranular boundaries leads to an increase in density, hardness, and mechanical strength of ceramics. The whole complex of properties of the synthesized material, with the addition of TiO(2) nanoparticles in the amount of 1.0–1.5 wt.%, leads to an increase in the ability to absorb electromagnetic radiation in the frequency range of electric current 8.2–12.4 GHz. The analysis and updating of knowledge on synthesis, and the investigation of properties of beryllium ceramics modified by nanoparticles, seems to be significant. The obtained results can be used in the creation of absorbers of scattered microwave radiation based on (BeO + TiO(2)) ceramics.
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spelling pubmed-105734732023-10-14 Synthesis and Investigation of Properties of Beryllium Ceramics Modified with Titanium Dioxide Nanoparticles Pavlov, Alexandr Sagdoldina, Zhuldyz Zhilkashinova, Almira Magazov, Nurtoleu Turar, Zhangabay Gert, Sergey Materials (Basel) Article Samples of beryllium ceramics, with the addition of micro- and nanoparticles TiO(2,) have been obtained by the method of thermoplastic slip casting. The microstructure of batch ceramics, consisting of micropowders and ceramics with TiO(2) nanoparticles sintered at an elevated temperature, has been investigated. It was found that the introduction of TiO(2) nanoparticles leads to changes in the mechanisms of mass transfer and microstructure formation, and the mobility of TiO(2) at interfacial grain boundaries increases, which leads to the formation of elements of a zonal shell structure. The reduction of intergranular boundaries leads to an increase in density, hardness, and mechanical strength of ceramics. The whole complex of properties of the synthesized material, with the addition of TiO(2) nanoparticles in the amount of 1.0–1.5 wt.%, leads to an increase in the ability to absorb electromagnetic radiation in the frequency range of electric current 8.2–12.4 GHz. The analysis and updating of knowledge on synthesis, and the investigation of properties of beryllium ceramics modified by nanoparticles, seems to be significant. The obtained results can be used in the creation of absorbers of scattered microwave radiation based on (BeO + TiO(2)) ceramics. MDPI 2023-09-30 /pmc/articles/PMC10573473/ /pubmed/37834644 http://dx.doi.org/10.3390/ma16196507 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Pavlov, Alexandr
Sagdoldina, Zhuldyz
Zhilkashinova, Almira
Magazov, Nurtoleu
Turar, Zhangabay
Gert, Sergey
Synthesis and Investigation of Properties of Beryllium Ceramics Modified with Titanium Dioxide Nanoparticles
title Synthesis and Investigation of Properties of Beryllium Ceramics Modified with Titanium Dioxide Nanoparticles
title_full Synthesis and Investigation of Properties of Beryllium Ceramics Modified with Titanium Dioxide Nanoparticles
title_fullStr Synthesis and Investigation of Properties of Beryllium Ceramics Modified with Titanium Dioxide Nanoparticles
title_full_unstemmed Synthesis and Investigation of Properties of Beryllium Ceramics Modified with Titanium Dioxide Nanoparticles
title_short Synthesis and Investigation of Properties of Beryllium Ceramics Modified with Titanium Dioxide Nanoparticles
title_sort synthesis and investigation of properties of beryllium ceramics modified with titanium dioxide nanoparticles
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10573473/
https://www.ncbi.nlm.nih.gov/pubmed/37834644
http://dx.doi.org/10.3390/ma16196507
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