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Effect of Aprotic Solvents on the Microtensile Bond Strength of Composite Core and Fiber-Reinforced Composite Posts
This investigation evaluated the effects of aprotic solvents, i.e., tetrahydrofuran, pyridine, and morpholine, compared with hydrogen peroxide, on the surfaces of fiber-reinforced composite posts with a composite core based on the microtensile bond strength. In total, 150 FRC Postec Plus posts and 1...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2023
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10574831/ https://www.ncbi.nlm.nih.gov/pubmed/37836032 http://dx.doi.org/10.3390/polym15193984 |
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author | Prawatvatchara, Wisarut Angkanawiriyarak, Somphote Klaisiri, Awiruth Sriamporn, Tool Thamrongananskul, Niyom |
author_facet | Prawatvatchara, Wisarut Angkanawiriyarak, Somphote Klaisiri, Awiruth Sriamporn, Tool Thamrongananskul, Niyom |
author_sort | Prawatvatchara, Wisarut |
collection | PubMed |
description | This investigation evaluated the effects of aprotic solvents, i.e., tetrahydrofuran, pyridine, and morpholine, compared with hydrogen peroxide, on the surfaces of fiber-reinforced composite posts with a composite core based on the microtensile bond strength. In total, 150 FRC Postec Plus posts and 150 D.T. Light-Posts were randomly divided into three groups (non-thermocycling, 5000-cycle, and 10,000-cycle thermocycling groups). Each group was divided into five subgroups according to the post-surface treatment: C, non-treatment group; H(2)O(2), immersed in 35% hydrogen peroxide; THF, immersed in tetrahydrofuran; PY, immersed in pyridine; and MP, immersed in morpholine. The treated specimens were placed in the bottom of a plastic cap and filled with a composite core material in preparation for the microtensile bond test. The data were evaluated using one-way ANOVA and Tukey’s test (p < 0.05) as well as an independent t-test (p < 0.05). For the surface roughness, white light interferometry was used for measurement, and the mean surface roughness was analyzed via one-way ANOVA and Tukey’s test (p < 0.05). The results showed that, under non-thermocycling conditions, the PY subgroup with D.T. Light-Post had the highest microtensile bond strength, followed by THF, MP, H(2)O(2), and the control groups. For FRC Postec Plus, the PY group had the highest microtensile bond strength, followed by MP, THF, H(2)O(2), and the control groups. Although the thermocycling conditions decreased the microtensile bond strength in all groups, the PY subgroup still had the highest value. An independent t-test revealed that even under all non-thermocycling and 5000- and 10,000-cycle thermocycling conditions, D.T. Light-Post in the PY subgroup displayed significantly higher microtensile bond strengths than FRC Postec Plus in the PY subgroup. While the surface roughness of the fiber-reinforced composite posts showed that the posts treated with pyridine possessed the highest surface roughness for each material type, In conclusion, as an aprotic solvent, pyridine generates the highest microtensile bond strength between the interfaces of composite cores and fiber-reinforced composite posts. |
format | Online Article Text |
id | pubmed-10574831 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2023 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-105748312023-10-14 Effect of Aprotic Solvents on the Microtensile Bond Strength of Composite Core and Fiber-Reinforced Composite Posts Prawatvatchara, Wisarut Angkanawiriyarak, Somphote Klaisiri, Awiruth Sriamporn, Tool Thamrongananskul, Niyom Polymers (Basel) Article This investigation evaluated the effects of aprotic solvents, i.e., tetrahydrofuran, pyridine, and morpholine, compared with hydrogen peroxide, on the surfaces of fiber-reinforced composite posts with a composite core based on the microtensile bond strength. In total, 150 FRC Postec Plus posts and 150 D.T. Light-Posts were randomly divided into three groups (non-thermocycling, 5000-cycle, and 10,000-cycle thermocycling groups). Each group was divided into five subgroups according to the post-surface treatment: C, non-treatment group; H(2)O(2), immersed in 35% hydrogen peroxide; THF, immersed in tetrahydrofuran; PY, immersed in pyridine; and MP, immersed in morpholine. The treated specimens were placed in the bottom of a plastic cap and filled with a composite core material in preparation for the microtensile bond test. The data were evaluated using one-way ANOVA and Tukey’s test (p < 0.05) as well as an independent t-test (p < 0.05). For the surface roughness, white light interferometry was used for measurement, and the mean surface roughness was analyzed via one-way ANOVA and Tukey’s test (p < 0.05). The results showed that, under non-thermocycling conditions, the PY subgroup with D.T. Light-Post had the highest microtensile bond strength, followed by THF, MP, H(2)O(2), and the control groups. For FRC Postec Plus, the PY group had the highest microtensile bond strength, followed by MP, THF, H(2)O(2), and the control groups. Although the thermocycling conditions decreased the microtensile bond strength in all groups, the PY subgroup still had the highest value. An independent t-test revealed that even under all non-thermocycling and 5000- and 10,000-cycle thermocycling conditions, D.T. Light-Post in the PY subgroup displayed significantly higher microtensile bond strengths than FRC Postec Plus in the PY subgroup. While the surface roughness of the fiber-reinforced composite posts showed that the posts treated with pyridine possessed the highest surface roughness for each material type, In conclusion, as an aprotic solvent, pyridine generates the highest microtensile bond strength between the interfaces of composite cores and fiber-reinforced composite posts. MDPI 2023-10-03 /pmc/articles/PMC10574831/ /pubmed/37836032 http://dx.doi.org/10.3390/polym15193984 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Prawatvatchara, Wisarut Angkanawiriyarak, Somphote Klaisiri, Awiruth Sriamporn, Tool Thamrongananskul, Niyom Effect of Aprotic Solvents on the Microtensile Bond Strength of Composite Core and Fiber-Reinforced Composite Posts |
title | Effect of Aprotic Solvents on the Microtensile Bond Strength of Composite Core and Fiber-Reinforced Composite Posts |
title_full | Effect of Aprotic Solvents on the Microtensile Bond Strength of Composite Core and Fiber-Reinforced Composite Posts |
title_fullStr | Effect of Aprotic Solvents on the Microtensile Bond Strength of Composite Core and Fiber-Reinforced Composite Posts |
title_full_unstemmed | Effect of Aprotic Solvents on the Microtensile Bond Strength of Composite Core and Fiber-Reinforced Composite Posts |
title_short | Effect of Aprotic Solvents on the Microtensile Bond Strength of Composite Core and Fiber-Reinforced Composite Posts |
title_sort | effect of aprotic solvents on the microtensile bond strength of composite core and fiber-reinforced composite posts |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10574831/ https://www.ncbi.nlm.nih.gov/pubmed/37836032 http://dx.doi.org/10.3390/polym15193984 |
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