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Ionic liquid immobilized on modified magnetic FSM-16: an efficient and magnetically recoverable nanocatalyst
In the present article, a nanocomposite was prepared by immobilizing ionic liquid on the magnetic mesoporous FSM-16 with a core–shell structure (Fe(3)O(4)@FSM-16-SO(3)/IL). Subsequently, the structural properties of the synthesized nanocatalyst were characterized and analyzed by various techniques s...
Autores principales: | , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
The Royal Society of Chemistry
2023
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Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10599354/ https://www.ncbi.nlm.nih.gov/pubmed/37886020 http://dx.doi.org/10.1039/d3ra04953a |
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author | Jahanbakhshi, Azar Farahi, Mahnaz |
author_facet | Jahanbakhshi, Azar Farahi, Mahnaz |
author_sort | Jahanbakhshi, Azar |
collection | PubMed |
description | In the present article, a nanocomposite was prepared by immobilizing ionic liquid on the magnetic mesoporous FSM-16 with a core–shell structure (Fe(3)O(4)@FSM-16-SO(3)/IL). Subsequently, the structural properties of the synthesized nanocatalyst were characterized and analyzed by various techniques such as XRD, FT-IR, TEM, FE-SEM, BET, VSM, TGA, and EDS. Fe(3)O(4)@FSM-16-SO(3)/IL was used as a recoverable and efficient nanocatalyst for the synthesis of polyhydroquinoline derivatives. The magnetic nanocatalyst showed remarkable stability and reusability and was reused six consecutive times without considerable loss of its activity. |
format | Online Article Text |
id | pubmed-10599354 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2023 |
publisher | The Royal Society of Chemistry |
record_format | MEDLINE/PubMed |
spelling | pubmed-105993542023-10-26 Ionic liquid immobilized on modified magnetic FSM-16: an efficient and magnetically recoverable nanocatalyst Jahanbakhshi, Azar Farahi, Mahnaz RSC Adv Chemistry In the present article, a nanocomposite was prepared by immobilizing ionic liquid on the magnetic mesoporous FSM-16 with a core–shell structure (Fe(3)O(4)@FSM-16-SO(3)/IL). Subsequently, the structural properties of the synthesized nanocatalyst were characterized and analyzed by various techniques such as XRD, FT-IR, TEM, FE-SEM, BET, VSM, TGA, and EDS. Fe(3)O(4)@FSM-16-SO(3)/IL was used as a recoverable and efficient nanocatalyst for the synthesis of polyhydroquinoline derivatives. The magnetic nanocatalyst showed remarkable stability and reusability and was reused six consecutive times without considerable loss of its activity. The Royal Society of Chemistry 2023-10-25 /pmc/articles/PMC10599354/ /pubmed/37886020 http://dx.doi.org/10.1039/d3ra04953a Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by/3.0/ |
spellingShingle | Chemistry Jahanbakhshi, Azar Farahi, Mahnaz Ionic liquid immobilized on modified magnetic FSM-16: an efficient and magnetically recoverable nanocatalyst |
title | Ionic liquid immobilized on modified magnetic FSM-16: an efficient and magnetically recoverable nanocatalyst |
title_full | Ionic liquid immobilized on modified magnetic FSM-16: an efficient and magnetically recoverable nanocatalyst |
title_fullStr | Ionic liquid immobilized on modified magnetic FSM-16: an efficient and magnetically recoverable nanocatalyst |
title_full_unstemmed | Ionic liquid immobilized on modified magnetic FSM-16: an efficient and magnetically recoverable nanocatalyst |
title_short | Ionic liquid immobilized on modified magnetic FSM-16: an efficient and magnetically recoverable nanocatalyst |
title_sort | ionic liquid immobilized on modified magnetic fsm-16: an efficient and magnetically recoverable nanocatalyst |
topic | Chemistry |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10599354/ https://www.ncbi.nlm.nih.gov/pubmed/37886020 http://dx.doi.org/10.1039/d3ra04953a |
work_keys_str_mv | AT jahanbakhshiazar ionicliquidimmobilizedonmodifiedmagneticfsm16anefficientandmagneticallyrecoverablenanocatalyst AT farahimahnaz ionicliquidimmobilizedonmodifiedmagneticfsm16anefficientandmagneticallyrecoverablenanocatalyst |