Cargando…

Unblocking Process of Complex Sulfur–Iron Scale Blockage in Sulfur-Bearing Gas Wells and Its Mechanism

[Image: see text] In this paper, through the establishment of a blockage analysis process, multistage weight loss method, and FT-IR, GC-MS, SEM, EDS, XRD and other characterization test means, it is clear that the scale sample is mainly organic material covered with complex and diverse sulfur and ir...

Descripción completa

Detalles Bibliográficos
Autores principales: Lv, Yabo, Ou, Jiaqiang, Fu, Haoran, Li, Juan, Luo, Zhifeng, Yang, Xiaodong, Zhao, Jinming, Yang, Tingting
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2023
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10620789/
https://www.ncbi.nlm.nih.gov/pubmed/37929105
http://dx.doi.org/10.1021/acsomega.3c04031
_version_ 1785130276626628608
author Lv, Yabo
Ou, Jiaqiang
Fu, Haoran
Li, Juan
Luo, Zhifeng
Yang, Xiaodong
Zhao, Jinming
Yang, Tingting
author_facet Lv, Yabo
Ou, Jiaqiang
Fu, Haoran
Li, Juan
Luo, Zhifeng
Yang, Xiaodong
Zhao, Jinming
Yang, Tingting
author_sort Lv, Yabo
collection PubMed
description [Image: see text] In this paper, through the establishment of a blockage analysis process, multistage weight loss method, and FT-IR, GC-MS, SEM, EDS, XRD and other characterization test means, it is clear that the scale sample is mainly organic material covered with complex and diverse sulfur and iron compounds, and the mechanism of sulfur-containing gas well blockage is revealed by tracing into the well material, formation minerals, acid gas corrosion, and other substances. Through the selection of chelating agent, cleaning agent, and acid concentration, as well as the optimization of different process parameters, the “dispersion-chelation-dissolution” composite unblocking technology is proposed, and a set of unblocking formula systems for complex sulfur and iron scale is clarified. Finally, XRD and SEM characterization tests of the scale samples before and after dissolution were conducted to study the declogging mechanism and confirm the acid-insoluble nature of FeS(2) and its stability in a weak acidic environment.
format Online
Article
Text
id pubmed-10620789
institution National Center for Biotechnology Information
language English
publishDate 2023
publisher American Chemical Society
record_format MEDLINE/PubMed
spelling pubmed-106207892023-11-03 Unblocking Process of Complex Sulfur–Iron Scale Blockage in Sulfur-Bearing Gas Wells and Its Mechanism Lv, Yabo Ou, Jiaqiang Fu, Haoran Li, Juan Luo, Zhifeng Yang, Xiaodong Zhao, Jinming Yang, Tingting ACS Omega [Image: see text] In this paper, through the establishment of a blockage analysis process, multistage weight loss method, and FT-IR, GC-MS, SEM, EDS, XRD and other characterization test means, it is clear that the scale sample is mainly organic material covered with complex and diverse sulfur and iron compounds, and the mechanism of sulfur-containing gas well blockage is revealed by tracing into the well material, formation minerals, acid gas corrosion, and other substances. Through the selection of chelating agent, cleaning agent, and acid concentration, as well as the optimization of different process parameters, the “dispersion-chelation-dissolution” composite unblocking technology is proposed, and a set of unblocking formula systems for complex sulfur and iron scale is clarified. Finally, XRD and SEM characterization tests of the scale samples before and after dissolution were conducted to study the declogging mechanism and confirm the acid-insoluble nature of FeS(2) and its stability in a weak acidic environment. American Chemical Society 2023-10-20 /pmc/articles/PMC10620789/ /pubmed/37929105 http://dx.doi.org/10.1021/acsomega.3c04031 Text en © 2023 The Authors. Published by American Chemical Society https://creativecommons.org/licenses/by-nc-nd/4.0/Permits non-commercial access and re-use, provided that author attribution and integrity are maintained; but does not permit creation of adaptations or other derivative works (https://creativecommons.org/licenses/by-nc-nd/4.0/).
spellingShingle Lv, Yabo
Ou, Jiaqiang
Fu, Haoran
Li, Juan
Luo, Zhifeng
Yang, Xiaodong
Zhao, Jinming
Yang, Tingting
Unblocking Process of Complex Sulfur–Iron Scale Blockage in Sulfur-Bearing Gas Wells and Its Mechanism
title Unblocking Process of Complex Sulfur–Iron Scale Blockage in Sulfur-Bearing Gas Wells and Its Mechanism
title_full Unblocking Process of Complex Sulfur–Iron Scale Blockage in Sulfur-Bearing Gas Wells and Its Mechanism
title_fullStr Unblocking Process of Complex Sulfur–Iron Scale Blockage in Sulfur-Bearing Gas Wells and Its Mechanism
title_full_unstemmed Unblocking Process of Complex Sulfur–Iron Scale Blockage in Sulfur-Bearing Gas Wells and Its Mechanism
title_short Unblocking Process of Complex Sulfur–Iron Scale Blockage in Sulfur-Bearing Gas Wells and Its Mechanism
title_sort unblocking process of complex sulfur–iron scale blockage in sulfur-bearing gas wells and its mechanism
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10620789/
https://www.ncbi.nlm.nih.gov/pubmed/37929105
http://dx.doi.org/10.1021/acsomega.3c04031
work_keys_str_mv AT lvyabo unblockingprocessofcomplexsulfurironscaleblockageinsulfurbearinggaswellsanditsmechanism
AT oujiaqiang unblockingprocessofcomplexsulfurironscaleblockageinsulfurbearinggaswellsanditsmechanism
AT fuhaoran unblockingprocessofcomplexsulfurironscaleblockageinsulfurbearinggaswellsanditsmechanism
AT lijuan unblockingprocessofcomplexsulfurironscaleblockageinsulfurbearinggaswellsanditsmechanism
AT luozhifeng unblockingprocessofcomplexsulfurironscaleblockageinsulfurbearinggaswellsanditsmechanism
AT yangxiaodong unblockingprocessofcomplexsulfurironscaleblockageinsulfurbearinggaswellsanditsmechanism
AT zhaojinming unblockingprocessofcomplexsulfurironscaleblockageinsulfurbearinggaswellsanditsmechanism
AT yangtingting unblockingprocessofcomplexsulfurironscaleblockageinsulfurbearinggaswellsanditsmechanism