Cargando…

A domestic pressure cooker mediated, facile autoclaving method for the synthesis of silver nanoparticles

As an alternative to an expensive hydrothermal reactor, in the current method a domestic pressure was used for the synthesis of silver nanoparticles (Ag NP) using tree gum, kondagogu as dual functional reductant and stabilizer by autoclaving. The formation of Ag NP was evaluated with colour transfor...

Descripción completa

Detalles Bibliográficos
Autor principal: Kora, Aruna Jyothi
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10622712/
https://www.ncbi.nlm.nih.gov/pubmed/37928108
http://dx.doi.org/10.1016/j.mex.2023.102438
_version_ 1785130601552019456
author Kora, Aruna Jyothi
author_facet Kora, Aruna Jyothi
author_sort Kora, Aruna Jyothi
collection PubMed
description As an alternative to an expensive hydrothermal reactor, in the current method a domestic pressure was used for the synthesis of silver nanoparticles (Ag NP) using tree gum, kondagogu as dual functional reductant and stabilizer by autoclaving. The formation of Ag NP was evaluated with colour transformation, UV-Visible spectroscopy (UV–Vis) and transmission electron microscopy. The formation of Ag NP by gum confirmed from the developed yellow coloration of the solution and the appearance of surface plasmon resonance peak at 408 nm in the UV–Vis. The produced NP were spherical, polydisperse, particle size ranged from 2.9–17.6 nm and the average particle size was 4.5 ± 3.1 nm. The developed method is useful for demonstration, gaining hands on experience and production of metal and metal oxide NP in resource limited small laboratories, rural colleges, startups etc. • Pressure cooker serves as an easily accessible, durable, inexpensive, electricity independent hydrothermal nanoparticle production vessel. • Autoclaving serves as a facile, ecofriendly, less energy consuming, one pot, green method with dual functional role of in situ nanoparticle synthesis and sterilization. • Production of intrinsically safe and sterile nanoparticles amenable for in vivo and in vitro biomedical applications.
format Online
Article
Text
id pubmed-10622712
institution National Center for Biotechnology Information
language English
publishDate 2023
publisher Elsevier
record_format MEDLINE/PubMed
spelling pubmed-106227122023-11-04 A domestic pressure cooker mediated, facile autoclaving method for the synthesis of silver nanoparticles Kora, Aruna Jyothi MethodsX Materials Science As an alternative to an expensive hydrothermal reactor, in the current method a domestic pressure was used for the synthesis of silver nanoparticles (Ag NP) using tree gum, kondagogu as dual functional reductant and stabilizer by autoclaving. The formation of Ag NP was evaluated with colour transformation, UV-Visible spectroscopy (UV–Vis) and transmission electron microscopy. The formation of Ag NP by gum confirmed from the developed yellow coloration of the solution and the appearance of surface plasmon resonance peak at 408 nm in the UV–Vis. The produced NP were spherical, polydisperse, particle size ranged from 2.9–17.6 nm and the average particle size was 4.5 ± 3.1 nm. The developed method is useful for demonstration, gaining hands on experience and production of metal and metal oxide NP in resource limited small laboratories, rural colleges, startups etc. • Pressure cooker serves as an easily accessible, durable, inexpensive, electricity independent hydrothermal nanoparticle production vessel. • Autoclaving serves as a facile, ecofriendly, less energy consuming, one pot, green method with dual functional role of in situ nanoparticle synthesis and sterilization. • Production of intrinsically safe and sterile nanoparticles amenable for in vivo and in vitro biomedical applications. Elsevier 2023-10-12 /pmc/articles/PMC10622712/ /pubmed/37928108 http://dx.doi.org/10.1016/j.mex.2023.102438 Text en © 2023 The Author https://creativecommons.org/licenses/by-nc-nd/4.0/This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
spellingShingle Materials Science
Kora, Aruna Jyothi
A domestic pressure cooker mediated, facile autoclaving method for the synthesis of silver nanoparticles
title A domestic pressure cooker mediated, facile autoclaving method for the synthesis of silver nanoparticles
title_full A domestic pressure cooker mediated, facile autoclaving method for the synthesis of silver nanoparticles
title_fullStr A domestic pressure cooker mediated, facile autoclaving method for the synthesis of silver nanoparticles
title_full_unstemmed A domestic pressure cooker mediated, facile autoclaving method for the synthesis of silver nanoparticles
title_short A domestic pressure cooker mediated, facile autoclaving method for the synthesis of silver nanoparticles
title_sort domestic pressure cooker mediated, facile autoclaving method for the synthesis of silver nanoparticles
topic Materials Science
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10622712/
https://www.ncbi.nlm.nih.gov/pubmed/37928108
http://dx.doi.org/10.1016/j.mex.2023.102438
work_keys_str_mv AT koraarunajyothi adomesticpressurecookermediatedfacileautoclavingmethodforthesynthesisofsilvernanoparticles
AT koraarunajyothi domesticpressurecookermediatedfacileautoclavingmethodforthesynthesisofsilvernanoparticles