4-(3-Chloro­anilino)benzoic acid

The title compound, C(13)H(10)ClNO(2), was synthesized by a Buchwald–Hartwig reaction and its crystal structure was investigated for the first time. Crystallization in a variety of solvents led to the discovery of one crystal form. High-quality single crystals were obtained by slow evaporation and t...

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Detalles Bibliográficos
Autores principales: Liu, Xiaoting, Long, Sihui
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10626612/
https://www.ncbi.nlm.nih.gov/pubmed/37937123
http://dx.doi.org/10.1107/S2414314623005989
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author Liu, Xiaoting
Long, Sihui
author_facet Liu, Xiaoting
Long, Sihui
author_sort Liu, Xiaoting
collection PubMed
description The title compound, C(13)H(10)ClNO(2), was synthesized by a Buchwald–Hartwig reaction and its crystal structure was investigated for the first time. Crystallization in a variety of solvents led to the discovery of one crystal form. High-quality single crystals were obtained by slow evaporation and the crystal structure was determined by single-crystal X-ray diffraction. The mol­ecules in the crystal structures are highly twisted [the dihedral angle between the aromatic rings is 34.66 (6)°] and pair up to form acid–acid dimers. [Image: see text]
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spelling pubmed-106266122023-11-07 4-(3-Chloro­anilino)benzoic acid Liu, Xiaoting Long, Sihui IUCrdata Data Reports The title compound, C(13)H(10)ClNO(2), was synthesized by a Buchwald–Hartwig reaction and its crystal structure was investigated for the first time. Crystallization in a variety of solvents led to the discovery of one crystal form. High-quality single crystals were obtained by slow evaporation and the crystal structure was determined by single-crystal X-ray diffraction. The mol­ecules in the crystal structures are highly twisted [the dihedral angle between the aromatic rings is 34.66 (6)°] and pair up to form acid–acid dimers. [Image: see text] International Union of Crystallography 2023-07-14 /pmc/articles/PMC10626612/ /pubmed/37937123 http://dx.doi.org/10.1107/S2414314623005989 Text en © Liu and Long 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Liu, Xiaoting
Long, Sihui
4-(3-Chloro­anilino)benzoic acid
title 4-(3-Chloro­anilino)benzoic acid
title_full 4-(3-Chloro­anilino)benzoic acid
title_fullStr 4-(3-Chloro­anilino)benzoic acid
title_full_unstemmed 4-(3-Chloro­anilino)benzoic acid
title_short 4-(3-Chloro­anilino)benzoic acid
title_sort 4-(3-chloro­anilino)benzoic acid
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10626612/
https://www.ncbi.nlm.nih.gov/pubmed/37937123
http://dx.doi.org/10.1107/S2414314623005989
work_keys_str_mv AT liuxiaoting 43chloroanilinobenzoicacid
AT longsihui 43chloroanilinobenzoicacid

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