Crystal structure of 4-(naphthalen-2-yl)-2-oxo-6-phenyl-1,2-di­hydro­pyridine-3-carbo­nitrile

The synthesis and crystal structure of the title compound, C(22)H(14)N(2)O, are described. The title compound was synthesized by a three-component one-pot reaction in DMSO involving chalcone, cyano­acetamide and elemental sulfur as catalyst. The compound was characterized by spectroscopic methods an...

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Autores principales: Bui, Thai Thanh Thu, Mac, Dinh Hung, Quang Trung, Pham, Pham, Chien Thang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10626956/
https://www.ncbi.nlm.nih.gov/pubmed/37936842
http://dx.doi.org/10.1107/S2056989023009180
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author Bui, Thai Thanh Thu
Mac, Dinh Hung
Quang Trung, Pham
Pham, Chien Thang
author_facet Bui, Thai Thanh Thu
Mac, Dinh Hung
Quang Trung, Pham
Pham, Chien Thang
author_sort Bui, Thai Thanh Thu
collection PubMed
description The synthesis and crystal structure of the title compound, C(22)H(14)N(2)O, are described. The title compound was synthesized by a three-component one-pot reaction in DMSO involving chalcone, cyano­acetamide and elemental sulfur as catalyst. The compound was characterized by spectroscopic methods and single-crystal X-ray diffraction. The structure consists of inversion-related dimers produced by N—H⋯O hydrogen bonding, which further inter­act through π–π contacts.
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spelling pubmed-106269562023-11-07 Crystal structure of 4-(naphthalen-2-yl)-2-oxo-6-phenyl-1,2-di­hydro­pyridine-3-carbo­nitrile Bui, Thai Thanh Thu Mac, Dinh Hung Quang Trung, Pham Pham, Chien Thang Acta Crystallogr E Crystallogr Commun Research Communications The synthesis and crystal structure of the title compound, C(22)H(14)N(2)O, are described. The title compound was synthesized by a three-component one-pot reaction in DMSO involving chalcone, cyano­acetamide and elemental sulfur as catalyst. The compound was characterized by spectroscopic methods and single-crystal X-ray diffraction. The structure consists of inversion-related dimers produced by N—H⋯O hydrogen bonding, which further inter­act through π–π contacts. International Union of Crystallography 2023-10-26 /pmc/articles/PMC10626956/ /pubmed/37936842 http://dx.doi.org/10.1107/S2056989023009180 Text en © Bui et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Communications
Bui, Thai Thanh Thu
Mac, Dinh Hung
Quang Trung, Pham
Pham, Chien Thang
Crystal structure of 4-(naphthalen-2-yl)-2-oxo-6-phenyl-1,2-di­hydro­pyridine-3-carbo­nitrile
title Crystal structure of 4-(naphthalen-2-yl)-2-oxo-6-phenyl-1,2-di­hydro­pyridine-3-carbo­nitrile
title_full Crystal structure of 4-(naphthalen-2-yl)-2-oxo-6-phenyl-1,2-di­hydro­pyridine-3-carbo­nitrile
title_fullStr Crystal structure of 4-(naphthalen-2-yl)-2-oxo-6-phenyl-1,2-di­hydro­pyridine-3-carbo­nitrile
title_full_unstemmed Crystal structure of 4-(naphthalen-2-yl)-2-oxo-6-phenyl-1,2-di­hydro­pyridine-3-carbo­nitrile
title_short Crystal structure of 4-(naphthalen-2-yl)-2-oxo-6-phenyl-1,2-di­hydro­pyridine-3-carbo­nitrile
title_sort crystal structure of 4-(naphthalen-2-yl)-2-oxo-6-phenyl-1,2-di­hydro­pyridine-3-carbo­nitrile
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10626956/
https://www.ncbi.nlm.nih.gov/pubmed/37936842
http://dx.doi.org/10.1107/S2056989023009180
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