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One-pot green bio-assisted synthesis of highly active catalytic palladium nanoparticles in porcine gastric mucin for environmental applications

In this work, palladium nanoparticles were synthesized using one-pot synthesis utilizing porcine gastric mucin glycoproteins as reducing and capping agents. It is shown that the particles exhibited noticeable catalytic activity through both nitrophenol reduction and Suzuki–Miyaura coupling reactions...

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Detalles Bibliográficos
Autores principales: Nudelman, Roman, Zuarets, Shir, Lev, Meiron, Gavriely, Shira, Meshi, Louisa, Zucker, Ines, Richter, Shachar
Formato: Online Artículo Texto
Lenguaje:English
Publicado: RSC 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10628991/
https://www.ncbi.nlm.nih.gov/pubmed/37941943
http://dx.doi.org/10.1039/d3na00385j
Descripción
Sumario:In this work, palladium nanoparticles were synthesized using one-pot synthesis utilizing porcine gastric mucin glycoproteins as reducing and capping agents. It is shown that the particles exhibited noticeable catalytic activity through both nitrophenol reduction and Suzuki–Miyaura coupling reactions. The catalytic performance was demonstrated with exceptionally high product yield, a fast reaction rate, and low catalyst use. The palladium–mucin composites obtained could be used in particle solution and as hydrogel catalysts to increase their reusability for at least ten reaction cycles with minimum loss in their catalytic effectiveness.