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One-pot green bio-assisted synthesis of highly active catalytic palladium nanoparticles in porcine gastric mucin for environmental applications

In this work, palladium nanoparticles were synthesized using one-pot synthesis utilizing porcine gastric mucin glycoproteins as reducing and capping agents. It is shown that the particles exhibited noticeable catalytic activity through both nitrophenol reduction and Suzuki–Miyaura coupling reactions...

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Detalles Bibliográficos
Autores principales: Nudelman, Roman, Zuarets, Shir, Lev, Meiron, Gavriely, Shira, Meshi, Louisa, Zucker, Ines, Richter, Shachar
Formato: Online Artículo Texto
Lenguaje:English
Publicado: RSC 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10628991/
https://www.ncbi.nlm.nih.gov/pubmed/37941943
http://dx.doi.org/10.1039/d3na00385j
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author Nudelman, Roman
Zuarets, Shir
Lev, Meiron
Gavriely, Shira
Meshi, Louisa
Zucker, Ines
Richter, Shachar
author_facet Nudelman, Roman
Zuarets, Shir
Lev, Meiron
Gavriely, Shira
Meshi, Louisa
Zucker, Ines
Richter, Shachar
author_sort Nudelman, Roman
collection PubMed
description In this work, palladium nanoparticles were synthesized using one-pot synthesis utilizing porcine gastric mucin glycoproteins as reducing and capping agents. It is shown that the particles exhibited noticeable catalytic activity through both nitrophenol reduction and Suzuki–Miyaura coupling reactions. The catalytic performance was demonstrated with exceptionally high product yield, a fast reaction rate, and low catalyst use. The palladium–mucin composites obtained could be used in particle solution and as hydrogel catalysts to increase their reusability for at least ten reaction cycles with minimum loss in their catalytic effectiveness.
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spelling pubmed-106289912023-11-08 One-pot green bio-assisted synthesis of highly active catalytic palladium nanoparticles in porcine gastric mucin for environmental applications Nudelman, Roman Zuarets, Shir Lev, Meiron Gavriely, Shira Meshi, Louisa Zucker, Ines Richter, Shachar Nanoscale Adv Chemistry In this work, palladium nanoparticles were synthesized using one-pot synthesis utilizing porcine gastric mucin glycoproteins as reducing and capping agents. It is shown that the particles exhibited noticeable catalytic activity through both nitrophenol reduction and Suzuki–Miyaura coupling reactions. The catalytic performance was demonstrated with exceptionally high product yield, a fast reaction rate, and low catalyst use. The palladium–mucin composites obtained could be used in particle solution and as hydrogel catalysts to increase their reusability for at least ten reaction cycles with minimum loss in their catalytic effectiveness. RSC 2023-09-07 /pmc/articles/PMC10628991/ /pubmed/37941943 http://dx.doi.org/10.1039/d3na00385j Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by-nc/3.0/
spellingShingle Chemistry
Nudelman, Roman
Zuarets, Shir
Lev, Meiron
Gavriely, Shira
Meshi, Louisa
Zucker, Ines
Richter, Shachar
One-pot green bio-assisted synthesis of highly active catalytic palladium nanoparticles in porcine gastric mucin for environmental applications
title One-pot green bio-assisted synthesis of highly active catalytic palladium nanoparticles in porcine gastric mucin for environmental applications
title_full One-pot green bio-assisted synthesis of highly active catalytic palladium nanoparticles in porcine gastric mucin for environmental applications
title_fullStr One-pot green bio-assisted synthesis of highly active catalytic palladium nanoparticles in porcine gastric mucin for environmental applications
title_full_unstemmed One-pot green bio-assisted synthesis of highly active catalytic palladium nanoparticles in porcine gastric mucin for environmental applications
title_short One-pot green bio-assisted synthesis of highly active catalytic palladium nanoparticles in porcine gastric mucin for environmental applications
title_sort one-pot green bio-assisted synthesis of highly active catalytic palladium nanoparticles in porcine gastric mucin for environmental applications
topic Chemistry
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10628991/
https://www.ncbi.nlm.nih.gov/pubmed/37941943
http://dx.doi.org/10.1039/d3na00385j
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