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SnAg(2)O(3)-Coated Adhesive Tape as a Recyclable Catalyst for Efficient Reduction of Methyl Orange

Silver oxide-doped tin oxide (SnAg(2)O(3)) nanoparticles were synthesized and different spectroscopic techniques were used to structurally identify SnAg(2)O(3) nanoparticles. The reduction of 4-nitrophenol (4-NP), congo red (CR), methylene blue (MB), and methyl orange (MO) was studied using SnAg(2)O...

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Autores principales: Akhtar, Kalsoom, Alhaj, Asma A., Bakhsh, Esraa M., Khan, Sher Bahadar, Fagieh, Taghreed M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10648674/
https://www.ncbi.nlm.nih.gov/pubmed/37959575
http://dx.doi.org/10.3390/ma16216978
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author Akhtar, Kalsoom
Alhaj, Asma A.
Bakhsh, Esraa M.
Khan, Sher Bahadar
Fagieh, Taghreed M.
author_facet Akhtar, Kalsoom
Alhaj, Asma A.
Bakhsh, Esraa M.
Khan, Sher Bahadar
Fagieh, Taghreed M.
author_sort Akhtar, Kalsoom
collection PubMed
description Silver oxide-doped tin oxide (SnAg(2)O(3)) nanoparticles were synthesized and different spectroscopic techniques were used to structurally identify SnAg(2)O(3) nanoparticles. The reduction of 4-nitrophenol (4-NP), congo red (CR), methylene blue (MB), and methyl orange (MO) was studied using SnAg(2)O(3) as a catalyst. Only 1.0 min was required to reduce 95% MO; thus, SnAg(2)O(3) was found to be effective with a rate constant of 3.0412 min(−1). Being a powder, SnAg(2)O(3) is difficult to recover and recycle multiple times. For this reason, SnAg(2)O(3) was coated on adhesive tape (AT) to make it recyclable for large-scale usage. SnAg(2)O(3)@AT catalyst was assessed toward MO reduction under various conditions. The amount of SnAg(2)O(3)@AT, NaBH(4), and MO was optimized for best possible reduction conditions. The catalyst had a positive effect since it speed up the reduction of MO by adding more SnAg(2)O(3)@AT and NaBH(4) as well as lowering the MO concentration. SnAg(2)O(3)@AT totally reduced MO (98%) in 3.0 min with a rate constant of 1.3669 min(−1). These findings confirmed that SnAg(2)O(3)@AT is an effective and useful catalyst for MO reduction that can even be utilized on a large scale for industrial purposes.
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spelling pubmed-106486742023-10-31 SnAg(2)O(3)-Coated Adhesive Tape as a Recyclable Catalyst for Efficient Reduction of Methyl Orange Akhtar, Kalsoom Alhaj, Asma A. Bakhsh, Esraa M. Khan, Sher Bahadar Fagieh, Taghreed M. Materials (Basel) Article Silver oxide-doped tin oxide (SnAg(2)O(3)) nanoparticles were synthesized and different spectroscopic techniques were used to structurally identify SnAg(2)O(3) nanoparticles. The reduction of 4-nitrophenol (4-NP), congo red (CR), methylene blue (MB), and methyl orange (MO) was studied using SnAg(2)O(3) as a catalyst. Only 1.0 min was required to reduce 95% MO; thus, SnAg(2)O(3) was found to be effective with a rate constant of 3.0412 min(−1). Being a powder, SnAg(2)O(3) is difficult to recover and recycle multiple times. For this reason, SnAg(2)O(3) was coated on adhesive tape (AT) to make it recyclable for large-scale usage. SnAg(2)O(3)@AT catalyst was assessed toward MO reduction under various conditions. The amount of SnAg(2)O(3)@AT, NaBH(4), and MO was optimized for best possible reduction conditions. The catalyst had a positive effect since it speed up the reduction of MO by adding more SnAg(2)O(3)@AT and NaBH(4) as well as lowering the MO concentration. SnAg(2)O(3)@AT totally reduced MO (98%) in 3.0 min with a rate constant of 1.3669 min(−1). These findings confirmed that SnAg(2)O(3)@AT is an effective and useful catalyst for MO reduction that can even be utilized on a large scale for industrial purposes. MDPI 2023-10-31 /pmc/articles/PMC10648674/ /pubmed/37959575 http://dx.doi.org/10.3390/ma16216978 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Akhtar, Kalsoom
Alhaj, Asma A.
Bakhsh, Esraa M.
Khan, Sher Bahadar
Fagieh, Taghreed M.
SnAg(2)O(3)-Coated Adhesive Tape as a Recyclable Catalyst for Efficient Reduction of Methyl Orange
title SnAg(2)O(3)-Coated Adhesive Tape as a Recyclable Catalyst for Efficient Reduction of Methyl Orange
title_full SnAg(2)O(3)-Coated Adhesive Tape as a Recyclable Catalyst for Efficient Reduction of Methyl Orange
title_fullStr SnAg(2)O(3)-Coated Adhesive Tape as a Recyclable Catalyst for Efficient Reduction of Methyl Orange
title_full_unstemmed SnAg(2)O(3)-Coated Adhesive Tape as a Recyclable Catalyst for Efficient Reduction of Methyl Orange
title_short SnAg(2)O(3)-Coated Adhesive Tape as a Recyclable Catalyst for Efficient Reduction of Methyl Orange
title_sort snag(2)o(3)-coated adhesive tape as a recyclable catalyst for efficient reduction of methyl orange
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10648674/
https://www.ncbi.nlm.nih.gov/pubmed/37959575
http://dx.doi.org/10.3390/ma16216978
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