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Fe(3)O(4)@void@C-Schiff-base/Pd yolk-shell nanostructures as an effective and reusable nanocatalyst for Suzuki coupling reaction

This article describes the synthesis of a novel Yolk-Shell structured Magnetic Yolk-Shell Nanomaterials Modified by Functionalized Carbon Shell with Schiff/Palladium Bases (Fe(3)O(4)@void@C-Schiff-base/Pd). The designed Fe(3)O(4)@void@C-Schiff-base/Pd catalyst was characterized using several techniq...

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Detalles Bibliográficos
Autores principales: Barzkar, Aliyeh, Salimi Beni, Alireza, Parang, Shahab, Salahshour, Farhang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10651923/
https://www.ncbi.nlm.nih.gov/pubmed/37968275
http://dx.doi.org/10.1038/s41598-023-46839-w
Descripción
Sumario:This article describes the synthesis of a novel Yolk-Shell structured Magnetic Yolk-Shell Nanomaterials Modified by Functionalized Carbon Shell with Schiff/Palladium Bases (Fe(3)O(4)@void@C-Schiff-base/Pd). The designed Fe(3)O(4)@void@C-Schiff-base/Pd catalyst was characterized using several techniques such as Fourier transform infrared spectroscopy (FTIR), vibrating sample magnetometry (VSM), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), thermal gravimetric analysis (TGA), powder X-ray diffraction (PXRD) and Inductively coupled plasma (ICP). The Fe(3)O(4)@void@C-Schiff-base/Pd was used as powerful catalyst for preparation Suzuki reaction in short reaction times and high yield in H(2)O at 60 °C and presence of potassium carbonate base. This nanocatalyst was magnetically recovered and reused several times with keeping its efficiency.