Fe(3)O(4)@void@C-Schiff-base/Pd yolk-shell nanostructures as an effective and reusable nanocatalyst for Suzuki coupling reaction

This article describes the synthesis of a novel Yolk-Shell structured Magnetic Yolk-Shell Nanomaterials Modified by Functionalized Carbon Shell with Schiff/Palladium Bases (Fe(3)O(4)@void@C-Schiff-base/Pd). The designed Fe(3)O(4)@void@C-Schiff-base/Pd catalyst was characterized using several techniq...

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Autores principales: Barzkar, Aliyeh, Salimi Beni, Alireza, Parang, Shahab, Salahshour, Farhang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2023
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10651923/
https://www.ncbi.nlm.nih.gov/pubmed/37968275
http://dx.doi.org/10.1038/s41598-023-46839-w
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author Barzkar, Aliyeh
Salimi Beni, Alireza
Parang, Shahab
Salahshour, Farhang
author_facet Barzkar, Aliyeh
Salimi Beni, Alireza
Parang, Shahab
Salahshour, Farhang
author_sort Barzkar, Aliyeh
collection PubMed
description This article describes the synthesis of a novel Yolk-Shell structured Magnetic Yolk-Shell Nanomaterials Modified by Functionalized Carbon Shell with Schiff/Palladium Bases (Fe(3)O(4)@void@C-Schiff-base/Pd). The designed Fe(3)O(4)@void@C-Schiff-base/Pd catalyst was characterized using several techniques such as Fourier transform infrared spectroscopy (FTIR), vibrating sample magnetometry (VSM), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), thermal gravimetric analysis (TGA), powder X-ray diffraction (PXRD) and Inductively coupled plasma (ICP). The Fe(3)O(4)@void@C-Schiff-base/Pd was used as powerful catalyst for preparation Suzuki reaction in short reaction times and high yield in H(2)O at 60 °C and presence of potassium carbonate base. This nanocatalyst was magnetically recovered and reused several times with keeping its efficiency.
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spelling pubmed-106519232023-11-15 Fe(3)O(4)@void@C-Schiff-base/Pd yolk-shell nanostructures as an effective and reusable nanocatalyst for Suzuki coupling reaction Barzkar, Aliyeh Salimi Beni, Alireza Parang, Shahab Salahshour, Farhang Sci Rep Article This article describes the synthesis of a novel Yolk-Shell structured Magnetic Yolk-Shell Nanomaterials Modified by Functionalized Carbon Shell with Schiff/Palladium Bases (Fe(3)O(4)@void@C-Schiff-base/Pd). The designed Fe(3)O(4)@void@C-Schiff-base/Pd catalyst was characterized using several techniques such as Fourier transform infrared spectroscopy (FTIR), vibrating sample magnetometry (VSM), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), thermal gravimetric analysis (TGA), powder X-ray diffraction (PXRD) and Inductively coupled plasma (ICP). The Fe(3)O(4)@void@C-Schiff-base/Pd was used as powerful catalyst for preparation Suzuki reaction in short reaction times and high yield in H(2)O at 60 °C and presence of potassium carbonate base. This nanocatalyst was magnetically recovered and reused several times with keeping its efficiency. Nature Publishing Group UK 2023-11-15 /pmc/articles/PMC10651923/ /pubmed/37968275 http://dx.doi.org/10.1038/s41598-023-46839-w Text en © The Author(s) 2023 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Article
Barzkar, Aliyeh
Salimi Beni, Alireza
Parang, Shahab
Salahshour, Farhang
Fe(3)O(4)@void@C-Schiff-base/Pd yolk-shell nanostructures as an effective and reusable nanocatalyst for Suzuki coupling reaction
title Fe(3)O(4)@void@C-Schiff-base/Pd yolk-shell nanostructures as an effective and reusable nanocatalyst for Suzuki coupling reaction
title_full Fe(3)O(4)@void@C-Schiff-base/Pd yolk-shell nanostructures as an effective and reusable nanocatalyst for Suzuki coupling reaction
title_fullStr Fe(3)O(4)@void@C-Schiff-base/Pd yolk-shell nanostructures as an effective and reusable nanocatalyst for Suzuki coupling reaction
title_full_unstemmed Fe(3)O(4)@void@C-Schiff-base/Pd yolk-shell nanostructures as an effective and reusable nanocatalyst for Suzuki coupling reaction
title_short Fe(3)O(4)@void@C-Schiff-base/Pd yolk-shell nanostructures as an effective and reusable nanocatalyst for Suzuki coupling reaction
title_sort fe(3)o(4)@void@c-schiff-base/pd yolk-shell nanostructures as an effective and reusable nanocatalyst for suzuki coupling reaction
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10651923/
https://www.ncbi.nlm.nih.gov/pubmed/37968275
http://dx.doi.org/10.1038/s41598-023-46839-w
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