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Micro-shear bond strength of different surface treatments on a polymer infiltrated ceramic network
Background: Polymer infiltrated ceramic networks, or hybrid ceramics, are a combination of infiltrating polymerizable organic monomers into a pre-sintered porous ceramic matrix. In addition to having good mechanical properties, the polymer infiltrated ceramic network must comply with the possibility...
Autores principales: | , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
F1000 Research Limited
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10665602/ https://www.ncbi.nlm.nih.gov/pubmed/37997604 http://dx.doi.org/10.12688/f1000research.122108.1 |
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author | Wahjuningrum, Dian Agustin Norberto, Calvo Ramírez Juan Fernanda, Méndez Mendieta Luisa Sari, Amanda Andika Pawar, Ajinkya M. Cruz González, Alberto Carlos |
author_facet | Wahjuningrum, Dian Agustin Norberto, Calvo Ramírez Juan Fernanda, Méndez Mendieta Luisa Sari, Amanda Andika Pawar, Ajinkya M. Cruz González, Alberto Carlos |
author_sort | Wahjuningrum, Dian Agustin |
collection | PubMed |
description | Background: Polymer infiltrated ceramic networks, or hybrid ceramics, are a combination of infiltrating polymerizable organic monomers into a pre-sintered porous ceramic matrix. In addition to having good mechanical properties, the polymer infiltrated ceramic network must comply with the possibility of adequate bonding to the resinous cement. The surface conditioning of this hybrid material must be carefully considered due to its organic composition and ceramic network. The purpose of this research is to evaluate the effect of hydrofluoric acid and a self-etching ceramic primer, under two different application times, on the bond strength of a polymer infiltrated ceramic network. Methods: Blocks of a polymer infiltrated ceramic network were cut to obtain sheets, and these were randomized into five groups. For the group termed AAS, airborne-particle abrasion with Al (2)O (3) (aluminum oxide) of 50µm was used. For groups HF2 and HF6, hydrofluoric acid was used for 20 and 60 seconds respectively, and for the groups MB2 and MB6, a self-etch ceramic primer was applied for 20 and 60 seconds respectively. A silane was applied to the groups AAS, HF2, and HF6 after the treatment. After 24-hour storage in distilled water, a micro-shear bond strength test was performed using a universal mechanical testing machine. All samples were evaluated in a stereomicroscope at 40x and 50x to determine the type of failure. Results: The highest and lowest values of bond strength were reported by groups MB6 and AAS, respectively. Groups HF2, HF6, MB6, and MB2 did not report statistically significant differences. The predominant failure pattern was a mixed failure. Conclusions: With the limitations of the present investigation, the treatments of self-etching ceramic primer and hydrofluoric acid followed by silane were reported to be statistically equal at 20 and 60 seconds. |
format | Online Article Text |
id | pubmed-10665602 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | F1000 Research Limited |
record_format | MEDLINE/PubMed |
spelling | pubmed-106656022022-07-18 Micro-shear bond strength of different surface treatments on a polymer infiltrated ceramic network Wahjuningrum, Dian Agustin Norberto, Calvo Ramírez Juan Fernanda, Méndez Mendieta Luisa Sari, Amanda Andika Pawar, Ajinkya M. Cruz González, Alberto Carlos F1000Res Research Article Background: Polymer infiltrated ceramic networks, or hybrid ceramics, are a combination of infiltrating polymerizable organic monomers into a pre-sintered porous ceramic matrix. In addition to having good mechanical properties, the polymer infiltrated ceramic network must comply with the possibility of adequate bonding to the resinous cement. The surface conditioning of this hybrid material must be carefully considered due to its organic composition and ceramic network. The purpose of this research is to evaluate the effect of hydrofluoric acid and a self-etching ceramic primer, under two different application times, on the bond strength of a polymer infiltrated ceramic network. Methods: Blocks of a polymer infiltrated ceramic network were cut to obtain sheets, and these were randomized into five groups. For the group termed AAS, airborne-particle abrasion with Al (2)O (3) (aluminum oxide) of 50µm was used. For groups HF2 and HF6, hydrofluoric acid was used for 20 and 60 seconds respectively, and for the groups MB2 and MB6, a self-etch ceramic primer was applied for 20 and 60 seconds respectively. A silane was applied to the groups AAS, HF2, and HF6 after the treatment. After 24-hour storage in distilled water, a micro-shear bond strength test was performed using a universal mechanical testing machine. All samples were evaluated in a stereomicroscope at 40x and 50x to determine the type of failure. Results: The highest and lowest values of bond strength were reported by groups MB6 and AAS, respectively. Groups HF2, HF6, MB6, and MB2 did not report statistically significant differences. The predominant failure pattern was a mixed failure. Conclusions: With the limitations of the present investigation, the treatments of self-etching ceramic primer and hydrofluoric acid followed by silane were reported to be statistically equal at 20 and 60 seconds. F1000 Research Limited 2022-07-18 /pmc/articles/PMC10665602/ /pubmed/37997604 http://dx.doi.org/10.12688/f1000research.122108.1 Text en Copyright: © 2022 Wahjuningrum DA et al. https://creativecommons.org/licenses/by/4.0/This is an open access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. |
spellingShingle | Research Article Wahjuningrum, Dian Agustin Norberto, Calvo Ramírez Juan Fernanda, Méndez Mendieta Luisa Sari, Amanda Andika Pawar, Ajinkya M. Cruz González, Alberto Carlos Micro-shear bond strength of different surface treatments on a polymer infiltrated ceramic network |
title | Micro-shear bond strength of different surface treatments on a polymer infiltrated ceramic network |
title_full | Micro-shear bond strength of different surface treatments on a polymer infiltrated ceramic network |
title_fullStr | Micro-shear bond strength of different surface treatments on a polymer infiltrated ceramic network |
title_full_unstemmed | Micro-shear bond strength of different surface treatments on a polymer infiltrated ceramic network |
title_short | Micro-shear bond strength of different surface treatments on a polymer infiltrated ceramic network |
title_sort | micro-shear bond strength of different surface treatments on a polymer infiltrated ceramic network |
topic | Research Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10665602/ https://www.ncbi.nlm.nih.gov/pubmed/37997604 http://dx.doi.org/10.12688/f1000research.122108.1 |
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