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Persistent Homology Analysis of the Microstructure of Laser-Powder-Bed-Fused Al–12Si Alloy

The laser powder bed fusion (L-PBF) process provides the cellular microstructure (primary α phase surrounded by a eutectic Si network) inside hypo-eutectic Al–Si alloys. The microstructure changes to the particle-dispersed microstructure with heat treatments at around 500 °C. The microstructural cha...

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Autores principales: Suzuki, Asuka, Sasa, Yusuke, Kobashi, Makoto, Kato, Masaki, Segawa, Masahito, Shimono, Yusuke, Nomoto, Sukeharu
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10673303/
https://www.ncbi.nlm.nih.gov/pubmed/38005157
http://dx.doi.org/10.3390/ma16227228
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author Suzuki, Asuka
Sasa, Yusuke
Kobashi, Makoto
Kato, Masaki
Segawa, Masahito
Shimono, Yusuke
Nomoto, Sukeharu
author_facet Suzuki, Asuka
Sasa, Yusuke
Kobashi, Makoto
Kato, Masaki
Segawa, Masahito
Shimono, Yusuke
Nomoto, Sukeharu
author_sort Suzuki, Asuka
collection PubMed
description The laser powder bed fusion (L-PBF) process provides the cellular microstructure (primary α phase surrounded by a eutectic Si network) inside hypo-eutectic Al–Si alloys. The microstructure changes to the particle-dispersed microstructure with heat treatments at around 500 °C. The microstructural change leads to a significant reduction in the tensile strength. However, the microstructural descriptors representing the cellular and particle-dispersed microstructures have not been established, resulting in difficulty in terms of discussion regarding the structure–property relationship. In this study, an attempt was made to analyze the microstructure in L-PBF-built and subsequently heat-treated Al–12Si (mass%) alloys using the persistent homology, which can analyze the spatial distributions and connections of secondary phases. The zero-dimensional persistent homology revealed that the spacing between adjacent Si particles was independent of Si particle size in the as-built alloy, whereas fewer Si particles existed near large Si particles in the heat-treated alloy. Furthermore, the first principal component of a one-dimensional persistent homology diagram would represent the microstructural characteristics from cellular to particle-dispersed morphology. These microstructural descriptors were strongly correlated with the tensile and yield strengths. This study provides a new insight into the microstructural indices describing unique microstructures in L-PBF-built alloys.
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spelling pubmed-106733032023-11-18 Persistent Homology Analysis of the Microstructure of Laser-Powder-Bed-Fused Al–12Si Alloy Suzuki, Asuka Sasa, Yusuke Kobashi, Makoto Kato, Masaki Segawa, Masahito Shimono, Yusuke Nomoto, Sukeharu Materials (Basel) Article The laser powder bed fusion (L-PBF) process provides the cellular microstructure (primary α phase surrounded by a eutectic Si network) inside hypo-eutectic Al–Si alloys. The microstructure changes to the particle-dispersed microstructure with heat treatments at around 500 °C. The microstructural change leads to a significant reduction in the tensile strength. However, the microstructural descriptors representing the cellular and particle-dispersed microstructures have not been established, resulting in difficulty in terms of discussion regarding the structure–property relationship. In this study, an attempt was made to analyze the microstructure in L-PBF-built and subsequently heat-treated Al–12Si (mass%) alloys using the persistent homology, which can analyze the spatial distributions and connections of secondary phases. The zero-dimensional persistent homology revealed that the spacing between adjacent Si particles was independent of Si particle size in the as-built alloy, whereas fewer Si particles existed near large Si particles in the heat-treated alloy. Furthermore, the first principal component of a one-dimensional persistent homology diagram would represent the microstructural characteristics from cellular to particle-dispersed morphology. These microstructural descriptors were strongly correlated with the tensile and yield strengths. This study provides a new insight into the microstructural indices describing unique microstructures in L-PBF-built alloys. MDPI 2023-11-18 /pmc/articles/PMC10673303/ /pubmed/38005157 http://dx.doi.org/10.3390/ma16227228 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Suzuki, Asuka
Sasa, Yusuke
Kobashi, Makoto
Kato, Masaki
Segawa, Masahito
Shimono, Yusuke
Nomoto, Sukeharu
Persistent Homology Analysis of the Microstructure of Laser-Powder-Bed-Fused Al–12Si Alloy
title Persistent Homology Analysis of the Microstructure of Laser-Powder-Bed-Fused Al–12Si Alloy
title_full Persistent Homology Analysis of the Microstructure of Laser-Powder-Bed-Fused Al–12Si Alloy
title_fullStr Persistent Homology Analysis of the Microstructure of Laser-Powder-Bed-Fused Al–12Si Alloy
title_full_unstemmed Persistent Homology Analysis of the Microstructure of Laser-Powder-Bed-Fused Al–12Si Alloy
title_short Persistent Homology Analysis of the Microstructure of Laser-Powder-Bed-Fused Al–12Si Alloy
title_sort persistent homology analysis of the microstructure of laser-powder-bed-fused al–12si alloy
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10673303/
https://www.ncbi.nlm.nih.gov/pubmed/38005157
http://dx.doi.org/10.3390/ma16227228
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