Cargando…
Green synthesis of quinazoline derivatives using a novel recyclable nano-catalyst of magnetic modified graphene oxide supported with copper
A new magnetic nano-catalyst system based on graphene oxide was designed and manufactured (GO@Fe(3)O(4)@3-chloropropyltrimethoxysilane@(Z)-N'-(2-hydroxybenzylidene)-4-(pyridin-4-yl)benzohydrazide@Cu(II)), and it was checked and confirmed by various analyzes such as FTIR, XRD, EDX, MAPPING, TGA/...
Autores principales: | , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Nature Publishing Group UK
2023
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10684527/ https://www.ncbi.nlm.nih.gov/pubmed/38017065 http://dx.doi.org/10.1038/s41598-023-48120-6 |
_version_ | 1785151420635283456 |
---|---|
author | Momeni, Sarieh Ghorbani‑Vaghei, Ramin |
author_facet | Momeni, Sarieh Ghorbani‑Vaghei, Ramin |
author_sort | Momeni, Sarieh |
collection | PubMed |
description | A new magnetic nano-catalyst system based on graphene oxide was designed and manufactured (GO@Fe(3)O(4)@3-chloropropyltrimethoxysilane@(Z)-N'-(2-hydroxybenzylidene)-4-(pyridin-4-yl)benzohydrazide@Cu(II)), and it was checked and confirmed by various analyzes such as FTIR, XRD, EDX, MAPPING, TGA/DSC, VSM and FESEM. This nano-catalyst was used in the three-component one-pot synthesis of quinazoline derivatives. The products were obtained using this efficient catalyst with high efficiency in short time and solvent-free conditions. Easy separation and acceptable recyclability are other advantages of this new nano-catalyst. Also, the catalyst can be recycled 4 times without a significant change in its efficiency. |
format | Online Article Text |
id | pubmed-10684527 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2023 |
publisher | Nature Publishing Group UK |
record_format | MEDLINE/PubMed |
spelling | pubmed-106845272023-11-30 Green synthesis of quinazoline derivatives using a novel recyclable nano-catalyst of magnetic modified graphene oxide supported with copper Momeni, Sarieh Ghorbani‑Vaghei, Ramin Sci Rep Article A new magnetic nano-catalyst system based on graphene oxide was designed and manufactured (GO@Fe(3)O(4)@3-chloropropyltrimethoxysilane@(Z)-N'-(2-hydroxybenzylidene)-4-(pyridin-4-yl)benzohydrazide@Cu(II)), and it was checked and confirmed by various analyzes such as FTIR, XRD, EDX, MAPPING, TGA/DSC, VSM and FESEM. This nano-catalyst was used in the three-component one-pot synthesis of quinazoline derivatives. The products were obtained using this efficient catalyst with high efficiency in short time and solvent-free conditions. Easy separation and acceptable recyclability are other advantages of this new nano-catalyst. Also, the catalyst can be recycled 4 times without a significant change in its efficiency. Nature Publishing Group UK 2023-11-28 /pmc/articles/PMC10684527/ /pubmed/38017065 http://dx.doi.org/10.1038/s41598-023-48120-6 Text en © The Author(s) 2023 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) . |
spellingShingle | Article Momeni, Sarieh Ghorbani‑Vaghei, Ramin Green synthesis of quinazoline derivatives using a novel recyclable nano-catalyst of magnetic modified graphene oxide supported with copper |
title | Green synthesis of quinazoline derivatives using a novel recyclable nano-catalyst of magnetic modified graphene oxide supported with copper |
title_full | Green synthesis of quinazoline derivatives using a novel recyclable nano-catalyst of magnetic modified graphene oxide supported with copper |
title_fullStr | Green synthesis of quinazoline derivatives using a novel recyclable nano-catalyst of magnetic modified graphene oxide supported with copper |
title_full_unstemmed | Green synthesis of quinazoline derivatives using a novel recyclable nano-catalyst of magnetic modified graphene oxide supported with copper |
title_short | Green synthesis of quinazoline derivatives using a novel recyclable nano-catalyst of magnetic modified graphene oxide supported with copper |
title_sort | green synthesis of quinazoline derivatives using a novel recyclable nano-catalyst of magnetic modified graphene oxide supported with copper |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10684527/ https://www.ncbi.nlm.nih.gov/pubmed/38017065 http://dx.doi.org/10.1038/s41598-023-48120-6 |
work_keys_str_mv | AT momenisarieh greensynthesisofquinazolinederivativesusinganovelrecyclablenanocatalystofmagneticmodifiedgrapheneoxidesupportedwithcopper AT ghorbanivagheiramin greensynthesisofquinazolinederivativesusinganovelrecyclablenanocatalystofmagneticmodifiedgrapheneoxidesupportedwithcopper |