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An introductory laboratory class in sonochemistry

This article proposes a substantive scope and scenario of a laboratory class that introduces students to the field of sonochemistry. The class requires only basic laboratory equipment - typical laboratory glassware like graduated pipettes and conical flasks, as well as simple inorganic chemicals. It...

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Autor principal: Matyszczak, Grzegorz
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10685300/
https://www.ncbi.nlm.nih.gov/pubmed/37976564
http://dx.doi.org/10.1016/j.ultsonch.2023.106691
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author Matyszczak, Grzegorz
author_facet Matyszczak, Grzegorz
author_sort Matyszczak, Grzegorz
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description This article proposes a substantive scope and scenario of a laboratory class that introduces students to the field of sonochemistry. The class requires only basic laboratory equipment - typical laboratory glassware like graduated pipettes and conical flasks, as well as simple inorganic chemicals. It is designed to acquaint students with fundamental aspects of sonochemistry. In the qualitative aspect, they will conduct and observe some sonochemical reactions like a synthesis of hydrogen peroxide and ultrasound-assisted degradation of toxic chromates(VI) which will demonstrate the indirect consequences of water sonolysis which is the most basic sonochemical reaction, as well as they will illustrate the applications of sonochemistry. In the quantitative aspect, students will learn about how to measure the power of ultrasound and the sonochemical efficiency of the reaction and will conduct experiments allowing for the calculation of these parameters. Finally, an introduction to and demonstration of the sonocatalytic effect is planned. An evaluation system, consisting of a report and test, is also proposed.
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spelling pubmed-106853002023-11-30 An introductory laboratory class in sonochemistry Matyszczak, Grzegorz Ultrason Sonochem Original Research Article This article proposes a substantive scope and scenario of a laboratory class that introduces students to the field of sonochemistry. The class requires only basic laboratory equipment - typical laboratory glassware like graduated pipettes and conical flasks, as well as simple inorganic chemicals. It is designed to acquaint students with fundamental aspects of sonochemistry. In the qualitative aspect, they will conduct and observe some sonochemical reactions like a synthesis of hydrogen peroxide and ultrasound-assisted degradation of toxic chromates(VI) which will demonstrate the indirect consequences of water sonolysis which is the most basic sonochemical reaction, as well as they will illustrate the applications of sonochemistry. In the quantitative aspect, students will learn about how to measure the power of ultrasound and the sonochemical efficiency of the reaction and will conduct experiments allowing for the calculation of these parameters. Finally, an introduction to and demonstration of the sonocatalytic effect is planned. An evaluation system, consisting of a report and test, is also proposed. Elsevier 2023-11-07 /pmc/articles/PMC10685300/ /pubmed/37976564 http://dx.doi.org/10.1016/j.ultsonch.2023.106691 Text en © 2023 The Author https://creativecommons.org/licenses/by/4.0/This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Original Research Article
Matyszczak, Grzegorz
An introductory laboratory class in sonochemistry
title An introductory laboratory class in sonochemistry
title_full An introductory laboratory class in sonochemistry
title_fullStr An introductory laboratory class in sonochemistry
title_full_unstemmed An introductory laboratory class in sonochemistry
title_short An introductory laboratory class in sonochemistry
title_sort introductory laboratory class in sonochemistry
topic Original Research Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10685300/
https://www.ncbi.nlm.nih.gov/pubmed/37976564
http://dx.doi.org/10.1016/j.ultsonch.2023.106691
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