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A method for generating uniform size-segregated pyrite particle fractions
BACKGROUND: Standardized sample preparation techniques allow comparison of pyrite dissolution experiments under diverse conditions. Our objective was to assess dry and wet sieving preparation methodologies, and to develop a reproducible technique that yields uniformly size-distributed material withi...
Autores principales: | , , , , |
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Formato: | Texto |
Lenguaje: | English |
Publicado: |
BioMed Central
2007
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2098762/ https://www.ncbi.nlm.nih.gov/pubmed/17927834 http://dx.doi.org/10.1186/1467-4866-8-9 |
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author | Wolfe, Amy L Liu, Ran Stewart, Brian W Capo, Rosemary C Dzombak, David A |
author_facet | Wolfe, Amy L Liu, Ran Stewart, Brian W Capo, Rosemary C Dzombak, David A |
author_sort | Wolfe, Amy L |
collection | PubMed |
description | BACKGROUND: Standardized sample preparation techniques allow comparison of pyrite dissolution experiments under diverse conditions. Our objective was to assess dry and wet sieving preparation methodologies, and to develop a reproducible technique that yields uniformly size-distributed material within a limited size range of interest. RESULTS: Here, we describe a wet sieving preparation method that successfully concentrates pyrite particles within a 44–75 μm diameter range. In addition, this technique does not require a post-processing cleanup step to remove adhering particles, as those particles are removed during the procedure. We show that sample preparation methods not only affect the pyrite size distribution, but also apparent dissolution rates. CONCLUSION: The presented methodology is non-destructive to the sample, uses readily available chemical equipment within the laboratory, and could be applied to minerals other than pyrite. |
format | Text |
id | pubmed-2098762 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2007 |
publisher | BioMed Central |
record_format | MEDLINE/PubMed |
spelling | pubmed-20987622007-11-29 A method for generating uniform size-segregated pyrite particle fractions Wolfe, Amy L Liu, Ran Stewart, Brian W Capo, Rosemary C Dzombak, David A Geochem Trans Methodology BACKGROUND: Standardized sample preparation techniques allow comparison of pyrite dissolution experiments under diverse conditions. Our objective was to assess dry and wet sieving preparation methodologies, and to develop a reproducible technique that yields uniformly size-distributed material within a limited size range of interest. RESULTS: Here, we describe a wet sieving preparation method that successfully concentrates pyrite particles within a 44–75 μm diameter range. In addition, this technique does not require a post-processing cleanup step to remove adhering particles, as those particles are removed during the procedure. We show that sample preparation methods not only affect the pyrite size distribution, but also apparent dissolution rates. CONCLUSION: The presented methodology is non-destructive to the sample, uses readily available chemical equipment within the laboratory, and could be applied to minerals other than pyrite. BioMed Central 2007-10-10 /pmc/articles/PMC2098762/ /pubmed/17927834 http://dx.doi.org/10.1186/1467-4866-8-9 Text en Copyright © 2007 Wolfe et al; licensee BioMed Central Ltd. http://creativecommons.org/licenses/by/2.0 This is an Open Access article distributed under the terms of the Creative Commons Attribution License ( (http://creativecommons.org/licenses/by/2.0) ), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. |
spellingShingle | Methodology Wolfe, Amy L Liu, Ran Stewart, Brian W Capo, Rosemary C Dzombak, David A A method for generating uniform size-segregated pyrite particle fractions |
title | A method for generating uniform size-segregated pyrite particle fractions |
title_full | A method for generating uniform size-segregated pyrite particle fractions |
title_fullStr | A method for generating uniform size-segregated pyrite particle fractions |
title_full_unstemmed | A method for generating uniform size-segregated pyrite particle fractions |
title_short | A method for generating uniform size-segregated pyrite particle fractions |
title_sort | method for generating uniform size-segregated pyrite particle fractions |
topic | Methodology |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2098762/ https://www.ncbi.nlm.nih.gov/pubmed/17927834 http://dx.doi.org/10.1186/1467-4866-8-9 |
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