Cargando…

Cost-effective upgrade of a focusing system for inelastic X-ray scattering experiments under high pressure

Inelastic X-ray scattering (IXS) is a powerful technique capable of probing the dynamic behavior and electronic structure of materials. For IXS experiments under high pressure up to the megabar range using state-of-the-art diamond-anvil-cell technology, the sample volume is limited to the order of 1...

Descripción completa

Detalles Bibliográficos
Autores principales: Huang, Chi-Yi, Cai, Yong Q., Hiraoka, Nozomu, Chen, Cheng-Chi, Chung, Shih-Chun, Song, Yen-Fang, Tsang, King-Long
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2467530/
https://www.ncbi.nlm.nih.gov/pubmed/18097078
http://dx.doi.org/10.1107/S0909049507055884
_version_ 1782157469693247488
author Huang, Chi-Yi
Cai, Yong Q.
Hiraoka, Nozomu
Chen, Cheng-Chi
Chung, Shih-Chun
Song, Yen-Fang
Tsang, King-Long
author_facet Huang, Chi-Yi
Cai, Yong Q.
Hiraoka, Nozomu
Chen, Cheng-Chi
Chung, Shih-Chun
Song, Yen-Fang
Tsang, King-Long
author_sort Huang, Chi-Yi
collection PubMed
description Inelastic X-ray scattering (IXS) is a powerful technique capable of probing the dynamic behavior and electronic structure of materials. For IXS experiments under high pressure up to the megabar range using state-of-the-art diamond-anvil-cell technology, the sample volume is limited to the order of 1 × 10(−3) mm(3) for which a beam focus of the same order and less is often required. In this paper a scheme utilizing a set of low-cost and compact Kirkpatrick–Baez mirrors for upgrading the existing optical system of the Taiwan IXS beamline at SPring-8 is described. The scheme as implemented improves the focus to 13 µm × 16 µm (horizontal × vertical) with a transmission of up to 72% and a flux density gain of over 30 times, which has enhanced substantially the efficiency of the beamline for high-pressure research.
format Text
id pubmed-2467530
institution National Center for Biotechnology Information
language English
publishDate 2008
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-24675302009-03-05 Cost-effective upgrade of a focusing system for inelastic X-ray scattering experiments under high pressure Huang, Chi-Yi Cai, Yong Q. Hiraoka, Nozomu Chen, Cheng-Chi Chung, Shih-Chun Song, Yen-Fang Tsang, King-Long J Synchrotron Radiat Research Papers Inelastic X-ray scattering (IXS) is a powerful technique capable of probing the dynamic behavior and electronic structure of materials. For IXS experiments under high pressure up to the megabar range using state-of-the-art diamond-anvil-cell technology, the sample volume is limited to the order of 1 × 10(−3) mm(3) for which a beam focus of the same order and less is often required. In this paper a scheme utilizing a set of low-cost and compact Kirkpatrick–Baez mirrors for upgrading the existing optical system of the Taiwan IXS beamline at SPring-8 is described. The scheme as implemented improves the focus to 13 µm × 16 µm (horizontal × vertical) with a transmission of up to 72% and a flux density gain of over 30 times, which has enhanced substantially the efficiency of the beamline for high-pressure research. International Union of Crystallography 2008-01-01 2007-12-18 /pmc/articles/PMC2467530/ /pubmed/18097078 http://dx.doi.org/10.1107/S0909049507055884 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Research Papers
Huang, Chi-Yi
Cai, Yong Q.
Hiraoka, Nozomu
Chen, Cheng-Chi
Chung, Shih-Chun
Song, Yen-Fang
Tsang, King-Long
Cost-effective upgrade of a focusing system for inelastic X-ray scattering experiments under high pressure
title Cost-effective upgrade of a focusing system for inelastic X-ray scattering experiments under high pressure
title_full Cost-effective upgrade of a focusing system for inelastic X-ray scattering experiments under high pressure
title_fullStr Cost-effective upgrade of a focusing system for inelastic X-ray scattering experiments under high pressure
title_full_unstemmed Cost-effective upgrade of a focusing system for inelastic X-ray scattering experiments under high pressure
title_short Cost-effective upgrade of a focusing system for inelastic X-ray scattering experiments under high pressure
title_sort cost-effective upgrade of a focusing system for inelastic x-ray scattering experiments under high pressure
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2467530/
https://www.ncbi.nlm.nih.gov/pubmed/18097078
http://dx.doi.org/10.1107/S0909049507055884
work_keys_str_mv AT huangchiyi costeffectiveupgradeofafocusingsystemforinelasticxrayscatteringexperimentsunderhighpressure
AT caiyongq costeffectiveupgradeofafocusingsystemforinelasticxrayscatteringexperimentsunderhighpressure
AT hiraokanozomu costeffectiveupgradeofafocusingsystemforinelasticxrayscatteringexperimentsunderhighpressure
AT chenchengchi costeffectiveupgradeofafocusingsystemforinelasticxrayscatteringexperimentsunderhighpressure
AT chungshihchun costeffectiveupgradeofafocusingsystemforinelasticxrayscatteringexperimentsunderhighpressure
AT songyenfang costeffectiveupgradeofafocusingsystemforinelasticxrayscatteringexperimentsunderhighpressure
AT tsangkinglong costeffectiveupgradeofafocusingsystemforinelasticxrayscatteringexperimentsunderhighpressure