Hydrostatic low-range pressure applications of the Paris–Edinburgh cell utilizing polymer gaskets for diffuse X-ray scattering measurements

The use of a polymeric Torlon (polyamide–imide) gasket material in a Paris–Edinburgh pressure cell for in situ high-pressure X-ray scattering measurements is demonstrated. The relatively low bulk modulus of the gasket allows for fine control of the sample pressure over the range 0.01–0.42 GPa. The q...

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Autores principales: Chapman, Karena W., Chupas, Peter J., Kurtz, Charles A., Locke, Darren R., Parise, John B., Hriljac, Joseph A.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Laboratory Notes
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2483494/
https://www.ncbi.nlm.nih.gov/pubmed/19461850
http://dx.doi.org/10.1107/S0021889806047923
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author Chapman, Karena W.
Chupas, Peter J.
Kurtz, Charles A.
Locke, Darren R.
Parise, John B.
Hriljac, Joseph A.
author_facet Chapman, Karena W.
Chupas, Peter J.
Kurtz, Charles A.
Locke, Darren R.
Parise, John B.
Hriljac, Joseph A.
author_sort Chapman, Karena W.
collection PubMed
description The use of a polymeric Torlon (polyamide–imide) gasket material in a Paris–Edinburgh pressure cell for in situ high-pressure X-ray scattering measurements is demonstrated. The relatively low bulk modulus of the gasket allows for fine control of the sample pressure over the range 0.01–0.42 GPa. The quality of the data obtained in this way is suitable for Bragg and pair distribution function analysis.
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spelling pubmed-24834942009-03-05 Hydrostatic low-range pressure applications of the Paris–Edinburgh cell utilizing polymer gaskets for diffuse X-ray scattering measurements Chapman, Karena W. Chupas, Peter J. Kurtz, Charles A. Locke, Darren R. Parise, John B. Hriljac, Joseph A. J Appl Crystallogr Laboratory Notes The use of a polymeric Torlon (polyamide–imide) gasket material in a Paris–Edinburgh pressure cell for in situ high-pressure X-ray scattering measurements is demonstrated. The relatively low bulk modulus of the gasket allows for fine control of the sample pressure over the range 0.01–0.42 GPa. The quality of the data obtained in this way is suitable for Bragg and pair distribution function analysis. International Union of Crystallography 2007-02-01 2007-01-12 /pmc/articles/PMC2483494/ /pubmed/19461850 http://dx.doi.org/10.1107/S0021889806047923 Text en © International Union of Crystallography 2007 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Laboratory Notes
Chapman, Karena W.
Chupas, Peter J.
Kurtz, Charles A.
Locke, Darren R.
Parise, John B.
Hriljac, Joseph A.
Hydrostatic low-range pressure applications of the Paris–Edinburgh cell utilizing polymer gaskets for diffuse X-ray scattering measurements
title Hydrostatic low-range pressure applications of the Paris–Edinburgh cell utilizing polymer gaskets for diffuse X-ray scattering measurements
title_full Hydrostatic low-range pressure applications of the Paris–Edinburgh cell utilizing polymer gaskets for diffuse X-ray scattering measurements
title_fullStr Hydrostatic low-range pressure applications of the Paris–Edinburgh cell utilizing polymer gaskets for diffuse X-ray scattering measurements
title_full_unstemmed Hydrostatic low-range pressure applications of the Paris–Edinburgh cell utilizing polymer gaskets for diffuse X-ray scattering measurements
title_short Hydrostatic low-range pressure applications of the Paris–Edinburgh cell utilizing polymer gaskets for diffuse X-ray scattering measurements
title_sort hydrostatic low-range pressure applications of the paris–edinburgh cell utilizing polymer gaskets for diffuse x-ray scattering measurements
topic Laboratory Notes
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2483494/
https://www.ncbi.nlm.nih.gov/pubmed/19461850
http://dx.doi.org/10.1107/S0021889806047923
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