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Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones
The solid-phase synthesis of 4H-3,1-benzoxazin-4-ones was achieved using silica-bound benzoyl chloride (SBBC) as dehydrating agent in reaction with 2-acylaminobenzoic acids. The silica-grafted reagent (SBBC) was simply recovered after reaction and reused several times.
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Formato: | Texto |
Lenguaje: | English |
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Beilstein-Institut
2009
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2686276/ https://www.ncbi.nlm.nih.gov/pubmed/19478965 http://dx.doi.org/10.3762/bjoc.5.13 |
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author | Rad-Moghadam, Kurosh Rouhi, Somayeh |
author_facet | Rad-Moghadam, Kurosh Rouhi, Somayeh |
author_sort | Rad-Moghadam, Kurosh |
collection | PubMed |
description | The solid-phase synthesis of 4H-3,1-benzoxazin-4-ones was achieved using silica-bound benzoyl chloride (SBBC) as dehydrating agent in reaction with 2-acylaminobenzoic acids. The silica-grafted reagent (SBBC) was simply recovered after reaction and reused several times. |
format | Text |
id | pubmed-2686276 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2009 |
publisher | Beilstein-Institut |
record_format | MEDLINE/PubMed |
spelling | pubmed-26862762009-05-28 Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones Rad-Moghadam, Kurosh Rouhi, Somayeh Beilstein J Org Chem Full Research Paper The solid-phase synthesis of 4H-3,1-benzoxazin-4-ones was achieved using silica-bound benzoyl chloride (SBBC) as dehydrating agent in reaction with 2-acylaminobenzoic acids. The silica-grafted reagent (SBBC) was simply recovered after reaction and reused several times. Beilstein-Institut 2009-04-23 /pmc/articles/PMC2686276/ /pubmed/19478965 http://dx.doi.org/10.3762/bjoc.5.13 Text en Copyright © 2009, Rad-Moghadam and Rouhi https://creativecommons.org/licenses/by/2.0https://www.beilstein-journals.org/bjoc/termsThis is an Open Access article under the terms of the Creative Commons Attribution License (https://creativecommons.org/licenses/by/2.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. The license is subject to the Beilstein Journal of Organic Chemistry terms and conditions: (https://www.beilstein-journals.org/bjoc/terms) |
spellingShingle | Full Research Paper Rad-Moghadam, Kurosh Rouhi, Somayeh Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones |
title | Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones |
title_full | Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones |
title_fullStr | Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones |
title_full_unstemmed | Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones |
title_short | Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones |
title_sort | silica-bound benzoyl chloride mediated the solid-phase synthesis of 4h-3,1-benzoxazin-4-ones |
topic | Full Research Paper |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2686276/ https://www.ncbi.nlm.nih.gov/pubmed/19478965 http://dx.doi.org/10.3762/bjoc.5.13 |
work_keys_str_mv | AT radmoghadamkurosh silicaboundbenzoylchloridemediatedthesolidphasesynthesisof4h31benzoxazin4ones AT rouhisomayeh silicaboundbenzoylchloridemediatedthesolidphasesynthesisof4h31benzoxazin4ones |