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Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones

The solid-phase synthesis of 4H-3,1-benzoxazin-4-ones was achieved using silica-bound benzoyl chloride (SBBC) as dehydrating agent in reaction with 2-acylaminobenzoic acids. The silica-grafted reagent (SBBC) was simply recovered after reaction and reused several times.

Detalles Bibliográficos
Autores principales: Rad-Moghadam, Kurosh, Rouhi, Somayeh
Formato: Texto
Lenguaje:English
Publicado: Beilstein-Institut 2009
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2686276/
https://www.ncbi.nlm.nih.gov/pubmed/19478965
http://dx.doi.org/10.3762/bjoc.5.13
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author Rad-Moghadam, Kurosh
Rouhi, Somayeh
author_facet Rad-Moghadam, Kurosh
Rouhi, Somayeh
author_sort Rad-Moghadam, Kurosh
collection PubMed
description The solid-phase synthesis of 4H-3,1-benzoxazin-4-ones was achieved using silica-bound benzoyl chloride (SBBC) as dehydrating agent in reaction with 2-acylaminobenzoic acids. The silica-grafted reagent (SBBC) was simply recovered after reaction and reused several times.
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spelling pubmed-26862762009-05-28 Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones Rad-Moghadam, Kurosh Rouhi, Somayeh Beilstein J Org Chem Full Research Paper The solid-phase synthesis of 4H-3,1-benzoxazin-4-ones was achieved using silica-bound benzoyl chloride (SBBC) as dehydrating agent in reaction with 2-acylaminobenzoic acids. The silica-grafted reagent (SBBC) was simply recovered after reaction and reused several times. Beilstein-Institut 2009-04-23 /pmc/articles/PMC2686276/ /pubmed/19478965 http://dx.doi.org/10.3762/bjoc.5.13 Text en Copyright © 2009, Rad-Moghadam and Rouhi https://creativecommons.org/licenses/by/2.0https://www.beilstein-journals.org/bjoc/termsThis is an Open Access article under the terms of the Creative Commons Attribution License (https://creativecommons.org/licenses/by/2.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. The license is subject to the Beilstein Journal of Organic Chemistry terms and conditions: (https://www.beilstein-journals.org/bjoc/terms)
spellingShingle Full Research Paper
Rad-Moghadam, Kurosh
Rouhi, Somayeh
Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones
title Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones
title_full Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones
title_fullStr Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones
title_full_unstemmed Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones
title_short Silica-bound benzoyl chloride mediated the solid-phase synthesis of 4H-3,1-benzoxazin-4-ones
title_sort silica-bound benzoyl chloride mediated the solid-phase synthesis of 4h-3,1-benzoxazin-4-ones
topic Full Research Paper
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2686276/
https://www.ncbi.nlm.nih.gov/pubmed/19478965
http://dx.doi.org/10.3762/bjoc.5.13
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