General methods for flash chromatography using disposable columns

As technology has evolved available guidelines for normal-phase flash chromatography have become less relevant. Years of experience performing chromatography with disposable columns have been condensed into simple guidelines useful for translating TLC results into either isocratic- or gradient-flash...

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Detalles Bibliográficos
Autores principales: Stevens, William C., Hill, Daniel C.
Formato: Texto
Lenguaje:English
Publicado: Springer Netherlands 2009
Materias:
Full Length Paper
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2780649/
https://www.ncbi.nlm.nih.gov/pubmed/19140020
http://dx.doi.org/10.1007/s11030-008-9104-x
Descripción
Sumario:As technology has evolved available guidelines for normal-phase flash chromatography have become less relevant. Years of experience performing chromatography with disposable columns have been condensed into simple guidelines useful for translating TLC results into either isocratic- or gradient-flash chromatography. The described studies should provide researchers with a means of selecting adequate columns and guidelines to reduce the waste of solvents, silica, time, and money. ELECTRONIC SUPPLEMENTARY MATERIAL: The online version of this article (doi:10.1007/s11030-008-9104-x) contains supplementary material, which is available to authorized users.

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