Solvent-free phase-vanishing reactions with PTFE (Teflon(®)) as a phase screen

In a solvent-free phase-vanishing reaction with PTFE (polytetrafluoroethylene, Teflon(®)) tape as the phase screen, a thermometer adapter is utilized to insert a PTFE-sealed tube into the vapor phase above the substrate. Besides avoiding use of solvents, the experimental design is not dependent upon...

Descripción completa

Detalles Bibliográficos
Autores principales: Pels, Kevin, Dragojlovic, Veljko
Formato: Texto
Lenguaje:English
Publicado: Beilstein-Institut 2009
Materias:
Preliminary Communication
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2839913/
https://www.ncbi.nlm.nih.gov/pubmed/20300472
http://dx.doi.org/10.3762/bjoc.5.75
Descripción
Sumario:In a solvent-free phase-vanishing reaction with PTFE (polytetrafluoroethylene, Teflon(®)) tape as the phase screen, a thermometer adapter is utilized to insert a PTFE-sealed tube into the vapor phase above the substrate. Besides avoiding use of solvents, the experimental design is not dependent upon the densities of the reactants and the procedure generates little or no waste while providing the reaction products in high yield and in high purity.

Ejemplares similares