Solvent-free phase-vanishing reactions with PTFE (Teflon(®)) as a phase screen

In a solvent-free phase-vanishing reaction with PTFE (polytetrafluoroethylene, Teflon(®)) tape as the phase screen, a thermometer adapter is utilized to insert a PTFE-sealed tube into the vapor phase above the substrate. Besides avoiding use of solvents, the experimental design is not dependent upon...

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Detalles Bibliográficos
Autores principales: Pels, Kevin, Dragojlovic, Veljko
Formato: Texto
Lenguaje:English
Publicado: Beilstein-Institut 2009
Materias:
Preliminary Communication
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2839913/
https://www.ncbi.nlm.nih.gov/pubmed/20300472
http://dx.doi.org/10.3762/bjoc.5.75
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author Pels, Kevin
Dragojlovic, Veljko
author_facet Pels, Kevin
Dragojlovic, Veljko
author_sort Pels, Kevin
collection PubMed
description In a solvent-free phase-vanishing reaction with PTFE (polytetrafluoroethylene, Teflon(®)) tape as the phase screen, a thermometer adapter is utilized to insert a PTFE-sealed tube into the vapor phase above the substrate. Besides avoiding use of solvents, the experimental design is not dependent upon the densities of the reactants and the procedure generates little or no waste while providing the reaction products in high yield and in high purity.
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spelling pubmed-28399132010-03-17 Solvent-free phase-vanishing reactions with PTFE (Teflon(®)) as a phase screen Pels, Kevin Dragojlovic, Veljko Beilstein J Org Chem Preliminary Communication In a solvent-free phase-vanishing reaction with PTFE (polytetrafluoroethylene, Teflon(®)) tape as the phase screen, a thermometer adapter is utilized to insert a PTFE-sealed tube into the vapor phase above the substrate. Besides avoiding use of solvents, the experimental design is not dependent upon the densities of the reactants and the procedure generates little or no waste while providing the reaction products in high yield and in high purity. Beilstein-Institut 2009-12-09 /pmc/articles/PMC2839913/ /pubmed/20300472 http://dx.doi.org/10.3762/bjoc.5.75 Text en Copyright © 2009, Pels and Dragojlovic https://creativecommons.org/licenses/by/2.0https://www.beilstein-journals.org/bjoc/termsThis is an Open Access article under the terms of the Creative Commons Attribution License (https://creativecommons.org/licenses/by/2.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. The license is subject to the Beilstein Journal of Organic Chemistry terms and conditions: (https://www.beilstein-journals.org/bjoc/terms)
spellingShingle Preliminary Communication
Pels, Kevin
Dragojlovic, Veljko
Solvent-free phase-vanishing reactions with PTFE (Teflon(®)) as a phase screen
title Solvent-free phase-vanishing reactions with PTFE (Teflon(®)) as a phase screen
title_full Solvent-free phase-vanishing reactions with PTFE (Teflon(®)) as a phase screen
title_fullStr Solvent-free phase-vanishing reactions with PTFE (Teflon(®)) as a phase screen
title_full_unstemmed Solvent-free phase-vanishing reactions with PTFE (Teflon(®)) as a phase screen
title_short Solvent-free phase-vanishing reactions with PTFE (Teflon(®)) as a phase screen
title_sort solvent-free phase-vanishing reactions with ptfe (teflon(®)) as a phase screen
topic Preliminary Communication
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2839913/
https://www.ncbi.nlm.nih.gov/pubmed/20300472
http://dx.doi.org/10.3762/bjoc.5.75
work_keys_str_mv AT pelskevin solventfreephasevanishingreactionswithptfeteflonasaphasescreen
AT dragojlovicveljko solventfreephasevanishingreactionswithptfeteflonasaphasescreen

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