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Trioctylphosphine as Both Solvent and Stabilizer to Synthesize CdS Nanorods
High quality CdS nanorods are synthesized reproducibly with cadmium acetate and sulfur as precursors in trioctylphosphine solution. The morphology, crystalline form and phase composition of CdS nanorods are characterized by transmission electron microscopy (TEM), high-resolution TEM and X-ray diffra...
Autores principales: | , , , |
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Formato: | Texto |
Lenguaje: | English |
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Springer
2009
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2893852/ https://www.ncbi.nlm.nih.gov/pubmed/20596487 http://dx.doi.org/10.1007/s11671-009-9375-x |
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author | Chen, Shutang Zhang, Xiaoling Zhang, Qiuhua Tan, Weihong |
author_facet | Chen, Shutang Zhang, Xiaoling Zhang, Qiuhua Tan, Weihong |
author_sort | Chen, Shutang |
collection | PubMed |
description | High quality CdS nanorods are synthesized reproducibly with cadmium acetate and sulfur as precursors in trioctylphosphine solution. The morphology, crystalline form and phase composition of CdS nanorods are characterized by transmission electron microscopy (TEM), high-resolution TEM and X-ray diffraction (XRD). CdS nanorods obtained are uniform with an aspect ratio of about 5:1 and in a wurtzite structure. The influence of reaction conditions on the growth of CdS nanorods demonstrates that low precursor concentration and high reaction temperature (260 °C) are favorable for the formation of uniform CdS nanorods with 85.3% of product yield. |
format | Text |
id | pubmed-2893852 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2009 |
publisher | Springer |
record_format | MEDLINE/PubMed |
spelling | pubmed-28938522010-06-30 Trioctylphosphine as Both Solvent and Stabilizer to Synthesize CdS Nanorods Chen, Shutang Zhang, Xiaoling Zhang, Qiuhua Tan, Weihong Nanoscale Res Lett Nano Express High quality CdS nanorods are synthesized reproducibly with cadmium acetate and sulfur as precursors in trioctylphosphine solution. The morphology, crystalline form and phase composition of CdS nanorods are characterized by transmission electron microscopy (TEM), high-resolution TEM and X-ray diffraction (XRD). CdS nanorods obtained are uniform with an aspect ratio of about 5:1 and in a wurtzite structure. The influence of reaction conditions on the growth of CdS nanorods demonstrates that low precursor concentration and high reaction temperature (260 °C) are favorable for the formation of uniform CdS nanorods with 85.3% of product yield. Springer 2009-06-17 /pmc/articles/PMC2893852/ /pubmed/20596487 http://dx.doi.org/10.1007/s11671-009-9375-x Text en Copyright ©2009 to the authors |
spellingShingle | Nano Express Chen, Shutang Zhang, Xiaoling Zhang, Qiuhua Tan, Weihong Trioctylphosphine as Both Solvent and Stabilizer to Synthesize CdS Nanorods |
title | Trioctylphosphine as Both Solvent and Stabilizer to Synthesize CdS Nanorods |
title_full | Trioctylphosphine as Both Solvent and Stabilizer to Synthesize CdS Nanorods |
title_fullStr | Trioctylphosphine as Both Solvent and Stabilizer to Synthesize CdS Nanorods |
title_full_unstemmed | Trioctylphosphine as Both Solvent and Stabilizer to Synthesize CdS Nanorods |
title_short | Trioctylphosphine as Both Solvent and Stabilizer to Synthesize CdS Nanorods |
title_sort | trioctylphosphine as both solvent and stabilizer to synthesize cds nanorods |
topic | Nano Express |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2893852/ https://www.ncbi.nlm.nih.gov/pubmed/20596487 http://dx.doi.org/10.1007/s11671-009-9375-x |
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