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Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves
A simple green approach for the production of benzylideneaniline oxides is offered. This contribution was performed via the condensation of phenylhydroxylamine with several aryl aldehydes, in the absence of both catalyst and solvent, and using microwave irradiation as the activating reaction mode. I...
Autores principales: | , , , , |
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Formato: | Texto |
Lenguaje: | English |
Publicado: |
Molecular Diversity Preservation International (MDPI)
2010
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2904933/ https://www.ncbi.nlm.nih.gov/pubmed/20640169 http://dx.doi.org/10.3390/ijms11062576 |
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author | Reyes, Leonor Corona, Sandra Arroyo, Gabriel Delgado, Francisco Miranda, René |
author_facet | Reyes, Leonor Corona, Sandra Arroyo, Gabriel Delgado, Francisco Miranda, René |
author_sort | Reyes, Leonor |
collection | PubMed |
description | A simple green approach for the production of benzylideneaniline oxides is offered. This contribution was performed via the condensation of phenylhydroxylamine with several aryl aldehydes, in the absence of both catalyst and solvent, and using microwave irradiation as the activating reaction mode. In addition, good yields of the products were achieved in a short time. It is also worth noting that the work-up procedure is simple and the products do not require further purification. Finally, an interesting comparison without the use of microwave irradiation is also discussed. |
format | Text |
id | pubmed-2904933 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2010 |
publisher | Molecular Diversity Preservation International (MDPI) |
record_format | MEDLINE/PubMed |
spelling | pubmed-29049332010-07-16 Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves Reyes, Leonor Corona, Sandra Arroyo, Gabriel Delgado, Francisco Miranda, René Int J Mol Sci Article A simple green approach for the production of benzylideneaniline oxides is offered. This contribution was performed via the condensation of phenylhydroxylamine with several aryl aldehydes, in the absence of both catalyst and solvent, and using microwave irradiation as the activating reaction mode. In addition, good yields of the products were achieved in a short time. It is also worth noting that the work-up procedure is simple and the products do not require further purification. Finally, an interesting comparison without the use of microwave irradiation is also discussed. Molecular Diversity Preservation International (MDPI) 2010-06-22 /pmc/articles/PMC2904933/ /pubmed/20640169 http://dx.doi.org/10.3390/ijms11062576 Text en © 2010 by the authors; licensee Molecular Diversity Preservation International, Basel, Switzerland. http://creativecommons.org/licenses/by/3.0 This article is an open-access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/3.0/). |
spellingShingle | Article Reyes, Leonor Corona, Sandra Arroyo, Gabriel Delgado, Francisco Miranda, René Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves |
title | Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves |
title_full | Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves |
title_fullStr | Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves |
title_full_unstemmed | Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves |
title_short | Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves |
title_sort | eco-contribution for the production of n-arylnitrones: solvent-free and assisted by microwaves |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2904933/ https://www.ncbi.nlm.nih.gov/pubmed/20640169 http://dx.doi.org/10.3390/ijms11062576 |
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