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Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves

A simple green approach for the production of benzylideneaniline oxides is offered. This contribution was performed via the condensation of phenylhydroxylamine with several aryl aldehydes, in the absence of both catalyst and solvent, and using microwave irradiation as the activating reaction mode. I...

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Detalles Bibliográficos
Autores principales: Reyes, Leonor, Corona, Sandra, Arroyo, Gabriel, Delgado, Francisco, Miranda, René
Formato: Texto
Lenguaje:English
Publicado: Molecular Diversity Preservation International (MDPI) 2010
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2904933/
https://www.ncbi.nlm.nih.gov/pubmed/20640169
http://dx.doi.org/10.3390/ijms11062576
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author Reyes, Leonor
Corona, Sandra
Arroyo, Gabriel
Delgado, Francisco
Miranda, René
author_facet Reyes, Leonor
Corona, Sandra
Arroyo, Gabriel
Delgado, Francisco
Miranda, René
author_sort Reyes, Leonor
collection PubMed
description A simple green approach for the production of benzylideneaniline oxides is offered. This contribution was performed via the condensation of phenylhydroxylamine with several aryl aldehydes, in the absence of both catalyst and solvent, and using microwave irradiation as the activating reaction mode. In addition, good yields of the products were achieved in a short time. It is also worth noting that the work-up procedure is simple and the products do not require further purification. Finally, an interesting comparison without the use of microwave irradiation is also discussed.
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spelling pubmed-29049332010-07-16 Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves Reyes, Leonor Corona, Sandra Arroyo, Gabriel Delgado, Francisco Miranda, René Int J Mol Sci Article A simple green approach for the production of benzylideneaniline oxides is offered. This contribution was performed via the condensation of phenylhydroxylamine with several aryl aldehydes, in the absence of both catalyst and solvent, and using microwave irradiation as the activating reaction mode. In addition, good yields of the products were achieved in a short time. It is also worth noting that the work-up procedure is simple and the products do not require further purification. Finally, an interesting comparison without the use of microwave irradiation is also discussed. Molecular Diversity Preservation International (MDPI) 2010-06-22 /pmc/articles/PMC2904933/ /pubmed/20640169 http://dx.doi.org/10.3390/ijms11062576 Text en © 2010 by the authors; licensee Molecular Diversity Preservation International, Basel, Switzerland. http://creativecommons.org/licenses/by/3.0 This article is an open-access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/3.0/).
spellingShingle Article
Reyes, Leonor
Corona, Sandra
Arroyo, Gabriel
Delgado, Francisco
Miranda, René
Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves
title Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves
title_full Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves
title_fullStr Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves
title_full_unstemmed Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves
title_short Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves
title_sort eco-contribution for the production of n-arylnitrones: solvent-free and assisted by microwaves
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2904933/
https://www.ncbi.nlm.nih.gov/pubmed/20640169
http://dx.doi.org/10.3390/ijms11062576
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