6-Oxobenz[de]isoquinolino[2,1-a]benzimidazolium chloride monohydrate

The title compound, C(18)H(11)N(2)O(+)·Cl(−)·H(2)O, was prepared by the reaction of 1,8-naphthalic anhydride with o-phenyl­ene­diamine in DMF. The dihedral angle formed by the phenyl and naphthalic rings is 177.06°. The structure is stabilized by intra­molecular C—H⋯O hydrogen bonds. There are N—H⋯C...

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Detalles Bibliográficos
Autores principales: Jian, Fang-Fang, Du, Li, Wang, Jing
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2914897/
https://www.ncbi.nlm.nih.gov/pubmed/21200947
http://dx.doi.org/10.1107/S1600536807061582
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author Jian, Fang-Fang
Du, Li
Wang, Jing
author_facet Jian, Fang-Fang
Du, Li
Wang, Jing
author_sort Jian, Fang-Fang
collection PubMed
description The title compound, C(18)H(11)N(2)O(+)·Cl(−)·H(2)O, was prepared by the reaction of 1,8-naphthalic anhydride with o-phenyl­ene­diamine in DMF. The dihedral angle formed by the phenyl and naphthalic rings is 177.06°. The structure is stabilized by intra­molecular C—H⋯O hydrogen bonds. There are N—H⋯Cl, O—H⋯Cl, C—H⋯O and C—H⋯Cl hydrogen bonds in the structure.
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spelling pubmed-29148972010-12-30 6-Oxobenz[de]isoquinolino[2,1-a]benzimidazolium chloride monohydrate Jian, Fang-Fang Du, Li Wang, Jing Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(18)H(11)N(2)O(+)·Cl(−)·H(2)O, was prepared by the reaction of 1,8-naphthalic anhydride with o-phenyl­ene­diamine in DMF. The dihedral angle formed by the phenyl and naphthalic rings is 177.06°. The structure is stabilized by intra­molecular C—H⋯O hydrogen bonds. There are N—H⋯Cl, O—H⋯Cl, C—H⋯O and C—H⋯Cl hydrogen bonds in the structure. International Union of Crystallography 2007-12-06 /pmc/articles/PMC2914897/ /pubmed/21200947 http://dx.doi.org/10.1107/S1600536807061582 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Jian, Fang-Fang
Du, Li
Wang, Jing
6-Oxobenz[de]isoquinolino[2,1-a]benzimidazolium chloride monohydrate
title 6-Oxobenz[de]isoquinolino[2,1-a]benzimidazolium chloride monohydrate
title_full 6-Oxobenz[de]isoquinolino[2,1-a]benzimidazolium chloride monohydrate
title_fullStr 6-Oxobenz[de]isoquinolino[2,1-a]benzimidazolium chloride monohydrate
title_full_unstemmed 6-Oxobenz[de]isoquinolino[2,1-a]benzimidazolium chloride monohydrate
title_short 6-Oxobenz[de]isoquinolino[2,1-a]benzimidazolium chloride monohydrate
title_sort 6-oxobenz[de]isoquinolino[2,1-a]benzimidazolium chloride monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2914897/
https://www.ncbi.nlm.nih.gov/pubmed/21200947
http://dx.doi.org/10.1107/S1600536807061582
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AT duli 6oxobenzdeisoquinolino21abenzimidazoliumchloridemonohydrate
AT wangjing 6oxobenzdeisoquinolino21abenzimidazoliumchloridemonohydrate

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