3-tert-Butyl-4-oxo-3,4-dihydro­phthalazin-1-yl 3,5-dimethyl­benzoate

The title compound, C(21)H(22)N(2)O(3), was synthesized by the reaction of tert-butyl­hydrazine with phthalic anhydride and further O-benzoyl­ation of the resulting inter­mediate by 3,5-dimethyl­benzoyl chloride. Inter­molecular C—H⋯O=C inter­actions link the mol­ecules into layers.

Detalles Bibliográficos
Autores principales: Wu, Dao-Xin, Chen, Zheng-Wang, Ren, Ye-Guo, Huang, Ming-Zhi
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2914898/
https://www.ncbi.nlm.nih.gov/pubmed/21200957
http://dx.doi.org/10.1107/S1600536807061089
_version_ 1782184811044012032
author Wu, Dao-Xin
Chen, Zheng-Wang
Ren, Ye-Guo
Huang, Ming-Zhi
author_facet Wu, Dao-Xin
Chen, Zheng-Wang
Ren, Ye-Guo
Huang, Ming-Zhi
author_sort Wu, Dao-Xin
collection PubMed
description The title compound, C(21)H(22)N(2)O(3), was synthesized by the reaction of tert-butyl­hydrazine with phthalic anhydride and further O-benzoyl­ation of the resulting inter­mediate by 3,5-dimethyl­benzoyl chloride. Inter­molecular C—H⋯O=C inter­actions link the mol­ecules into layers.
format Text
id pubmed-2914898
institution National Center for Biotechnology Information
language English
publishDate 2007
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29148982010-12-30 3-tert-Butyl-4-oxo-3,4-dihydro­phthalazin-1-yl 3,5-dimethyl­benzoate Wu, Dao-Xin Chen, Zheng-Wang Ren, Ye-Guo Huang, Ming-Zhi Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(21)H(22)N(2)O(3), was synthesized by the reaction of tert-butyl­hydrazine with phthalic anhydride and further O-benzoyl­ation of the resulting inter­mediate by 3,5-dimethyl­benzoyl chloride. Inter­molecular C—H⋯O=C inter­actions link the mol­ecules into layers. International Union of Crystallography 2007-12-06 /pmc/articles/PMC2914898/ /pubmed/21200957 http://dx.doi.org/10.1107/S1600536807061089 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Wu, Dao-Xin
Chen, Zheng-Wang
Ren, Ye-Guo
Huang, Ming-Zhi
3-tert-Butyl-4-oxo-3,4-dihydro­phthalazin-1-yl 3,5-dimethyl­benzoate
title 3-tert-Butyl-4-oxo-3,4-dihydro­phthalazin-1-yl 3,5-dimethyl­benzoate
title_full 3-tert-Butyl-4-oxo-3,4-dihydro­phthalazin-1-yl 3,5-dimethyl­benzoate
title_fullStr 3-tert-Butyl-4-oxo-3,4-dihydro­phthalazin-1-yl 3,5-dimethyl­benzoate
title_full_unstemmed 3-tert-Butyl-4-oxo-3,4-dihydro­phthalazin-1-yl 3,5-dimethyl­benzoate
title_short 3-tert-Butyl-4-oxo-3,4-dihydro­phthalazin-1-yl 3,5-dimethyl­benzoate
title_sort 3-tert-butyl-4-oxo-3,4-dihydro­phthalazin-1-yl 3,5-dimethyl­benzoate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2914898/
https://www.ncbi.nlm.nih.gov/pubmed/21200957
http://dx.doi.org/10.1107/S1600536807061089
work_keys_str_mv AT wudaoxin 3tertbutyl4oxo34dihydrophthalazin1yl35dimethylbenzoate
AT chenzhengwang 3tertbutyl4oxo34dihydrophthalazin1yl35dimethylbenzoate
AT renyeguo 3tertbutyl4oxo34dihydrophthalazin1yl35dimethylbenzoate
AT huangmingzhi 3tertbutyl4oxo34dihydrophthalazin1yl35dimethylbenzoate

Ejemplares similares