(E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N,N-diphenyl­cyclo­propane­carboxamide

The title compound, C(21)H(19)ClF(3)NO, was synthesized from 3-[(E)-2-chloro-3,3,3-trifluoro­prop-1-en­yl]-2,2-dimethyl­cyclo­propane­carboxylic acid and diphenyl­amine. The propenyl and carboxamide substituents lie on the same side of the cyclo­propane ring plane, with the two methyl substituents o...

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Detalles Bibliográficos
Autores principales: Yan, Fan-Yong, Liu, Dong-Qing
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2914980/
https://www.ncbi.nlm.nih.gov/pubmed/21200743
http://dx.doi.org/10.1107/S1600536807060953
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author Yan, Fan-Yong
Liu, Dong-Qing
author_facet Yan, Fan-Yong
Liu, Dong-Qing
author_sort Yan, Fan-Yong
collection PubMed
description The title compound, C(21)H(19)ClF(3)NO, was synthesized from 3-[(E)-2-chloro-3,3,3-trifluoro­prop-1-en­yl]-2,2-dimethyl­cyclo­propane­carboxylic acid and diphenyl­amine. The propenyl and carboxamide substituents lie on the same side of the cyclo­propane ring plane, with the two methyl substituents on either side of the plane. The phenyl rings of the carboxamide are inclined at an angle of 84.6 (3)° to one another. The F atoms are disordered over two positions; the site occupancy factors are ca 0.6 and 0.4.
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spelling pubmed-29149802010-12-30 (E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N,N-diphenyl­cyclo­propane­carboxamide Yan, Fan-Yong Liu, Dong-Qing Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(21)H(19)ClF(3)NO, was synthesized from 3-[(E)-2-chloro-3,3,3-trifluoro­prop-1-en­yl]-2,2-dimethyl­cyclo­propane­carboxylic acid and diphenyl­amine. The propenyl and carboxamide substituents lie on the same side of the cyclo­propane ring plane, with the two methyl substituents on either side of the plane. The phenyl rings of the carboxamide are inclined at an angle of 84.6 (3)° to one another. The F atoms are disordered over two positions; the site occupancy factors are ca 0.6 and 0.4. International Union of Crystallography 2007-12-06 /pmc/articles/PMC2914980/ /pubmed/21200743 http://dx.doi.org/10.1107/S1600536807060953 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Yan, Fan-Yong
Liu, Dong-Qing
(E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N,N-diphenyl­cyclo­propane­carboxamide
title (E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N,N-diphenyl­cyclo­propane­carboxamide
title_full (E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N,N-diphenyl­cyclo­propane­carboxamide
title_fullStr (E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N,N-diphenyl­cyclo­propane­carboxamide
title_full_unstemmed (E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N,N-diphenyl­cyclo­propane­carboxamide
title_short (E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N,N-diphenyl­cyclo­propane­carboxamide
title_sort (e)-3-(2-chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-n,n-diphenyl­cyclo­propane­carboxamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2914980/
https://www.ncbi.nlm.nih.gov/pubmed/21200743
http://dx.doi.org/10.1107/S1600536807060953
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AT liudongqing e32chloro333trifluoroprop1enyl22dimethylnndiphenylcyclopropanecarboxamide

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