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2-O-Benzhydryl-3,4-(S)-O-benzylidene-d-lyxono-1,4-lactone
X-ray crystallography unequivocally showed that protection of the free hydroxyl group of 3,5-O-benzylidene-d-lyxono-1,4-lactone with diphenyldiazomethane proceeded with retention of configuration to give the title compound, C(25)H(22)O(5). The crystal structure consists of layers of interlocked...
Autores principales: | , , , , , |
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Formato: | Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2008
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2914987/ https://www.ncbi.nlm.nih.gov/pubmed/21200976 http://dx.doi.org/10.1107/S1600536807059739 |
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author | Jenkinson, Sarah F. Rule, Sebastian D. Booth, Kathrine V. Fleet, George W. J. Watkin, David J. Petursson, Sigthor |
author_facet | Jenkinson, Sarah F. Rule, Sebastian D. Booth, Kathrine V. Fleet, George W. J. Watkin, David J. Petursson, Sigthor |
author_sort | Jenkinson, Sarah F. |
collection | PubMed |
description | X-ray crystallography unequivocally showed that protection of the free hydroxyl group of 3,5-O-benzylidene-d-lyxono-1,4-lactone with diphenyldiazomethane proceeded with retention of configuration to give the title compound, C(25)H(22)O(5). The crystal structure consists of layers of interlocked molecules lying parallel to the a axis. |
format | Text |
id | pubmed-2914987 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2008 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29149872010-12-30 2-O-Benzhydryl-3,4-(S)-O-benzylidene-d-lyxono-1,4-lactone Jenkinson, Sarah F. Rule, Sebastian D. Booth, Kathrine V. Fleet, George W. J. Watkin, David J. Petursson, Sigthor Acta Crystallogr Sect E Struct Rep Online Organic Papers X-ray crystallography unequivocally showed that protection of the free hydroxyl group of 3,5-O-benzylidene-d-lyxono-1,4-lactone with diphenyldiazomethane proceeded with retention of configuration to give the title compound, C(25)H(22)O(5). The crystal structure consists of layers of interlocked molecules lying parallel to the a axis. International Union of Crystallography 2008-12-06 /pmc/articles/PMC2914987/ /pubmed/21200976 http://dx.doi.org/10.1107/S1600536807059739 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html. |
spellingShingle | Organic Papers Jenkinson, Sarah F. Rule, Sebastian D. Booth, Kathrine V. Fleet, George W. J. Watkin, David J. Petursson, Sigthor 2-O-Benzhydryl-3,4-(S)-O-benzylidene-d-lyxono-1,4-lactone |
title | 2-O-Benzhydryl-3,4-(S)-O-benzylidene-d-lyxono-1,4-lactone |
title_full | 2-O-Benzhydryl-3,4-(S)-O-benzylidene-d-lyxono-1,4-lactone |
title_fullStr | 2-O-Benzhydryl-3,4-(S)-O-benzylidene-d-lyxono-1,4-lactone |
title_full_unstemmed | 2-O-Benzhydryl-3,4-(S)-O-benzylidene-d-lyxono-1,4-lactone |
title_short | 2-O-Benzhydryl-3,4-(S)-O-benzylidene-d-lyxono-1,4-lactone |
title_sort | 2-o-benzhydryl-3,4-(s)-o-benzylidene-d-lyxono-1,4-lactone |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2914987/ https://www.ncbi.nlm.nih.gov/pubmed/21200976 http://dx.doi.org/10.1107/S1600536807059739 |
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