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2-O-Benzhydryl-3,4-(S)-O-benzyl­idene-d-lyxono-1,4-lactone

X-ray crystallography unequivocally showed that protection of the free hydroxyl group of 3,5-O-benzyl­idene-d-lyxono-1,4-lactone with diphenyl­diazo­methane proceeded with retention of configuration to give the title compound, C(25)H(22)O(5). The crystal structure consists of layers of inter­locked...

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Detalles Bibliográficos
Autores principales: Jenkinson, Sarah F., Rule, Sebastian D., Booth, Kathrine V., Fleet, George W. J., Watkin, David J., Petursson, Sigthor
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2914987/
https://www.ncbi.nlm.nih.gov/pubmed/21200976
http://dx.doi.org/10.1107/S1600536807059739
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author Jenkinson, Sarah F.
Rule, Sebastian D.
Booth, Kathrine V.
Fleet, George W. J.
Watkin, David J.
Petursson, Sigthor
author_facet Jenkinson, Sarah F.
Rule, Sebastian D.
Booth, Kathrine V.
Fleet, George W. J.
Watkin, David J.
Petursson, Sigthor
author_sort Jenkinson, Sarah F.
collection PubMed
description X-ray crystallography unequivocally showed that protection of the free hydroxyl group of 3,5-O-benzyl­idene-d-lyxono-1,4-lactone with diphenyl­diazo­methane proceeded with retention of configuration to give the title compound, C(25)H(22)O(5). The crystal structure consists of layers of inter­locked mol­ecules lying parallel to the a axis.
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spelling pubmed-29149872010-12-30 2-O-Benzhydryl-3,4-(S)-O-benzyl­idene-d-lyxono-1,4-lactone Jenkinson, Sarah F. Rule, Sebastian D. Booth, Kathrine V. Fleet, George W. J. Watkin, David J. Petursson, Sigthor Acta Crystallogr Sect E Struct Rep Online Organic Papers X-ray crystallography unequivocally showed that protection of the free hydroxyl group of 3,5-O-benzyl­idene-d-lyxono-1,4-lactone with diphenyl­diazo­methane proceeded with retention of configuration to give the title compound, C(25)H(22)O(5). The crystal structure consists of layers of inter­locked mol­ecules lying parallel to the a axis. International Union of Crystallography 2008-12-06 /pmc/articles/PMC2914987/ /pubmed/21200976 http://dx.doi.org/10.1107/S1600536807059739 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Jenkinson, Sarah F.
Rule, Sebastian D.
Booth, Kathrine V.
Fleet, George W. J.
Watkin, David J.
Petursson, Sigthor
2-O-Benzhydryl-3,4-(S)-O-benzyl­idene-d-lyxono-1,4-lactone
title 2-O-Benzhydryl-3,4-(S)-O-benzyl­idene-d-lyxono-1,4-lactone
title_full 2-O-Benzhydryl-3,4-(S)-O-benzyl­idene-d-lyxono-1,4-lactone
title_fullStr 2-O-Benzhydryl-3,4-(S)-O-benzyl­idene-d-lyxono-1,4-lactone
title_full_unstemmed 2-O-Benzhydryl-3,4-(S)-O-benzyl­idene-d-lyxono-1,4-lactone
title_short 2-O-Benzhydryl-3,4-(S)-O-benzyl­idene-d-lyxono-1,4-lactone
title_sort 2-o-benzhydryl-3,4-(s)-o-benzyl­idene-d-lyxono-1,4-lactone
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2914987/
https://www.ncbi.nlm.nih.gov/pubmed/21200976
http://dx.doi.org/10.1107/S1600536807059739
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