1,4-Bis(piperidin-1-ylcarbon­yl)benzene

The title compound, C(18)H(20)N(2)O(2), has been synthesized by the reaction of terephthaloyl chloride and 1,2,3,6-tetra­hydro­pyridine. This compound crystallizes as discrete mol­ecular species disposed about a crystallographic centre of symmetry, such that half the mol­ecule constitutes the asymme...

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Detalles Bibliográficos
Autores principales: Armbrust, Lee, Bilyk, Alex, Brown, Christopher L., Healy, Peter C.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2914991/
https://www.ncbi.nlm.nih.gov/pubmed/21200873
http://dx.doi.org/10.1107/S1600536807062423
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author Armbrust, Lee
Bilyk, Alex
Brown, Christopher L.
Healy, Peter C.
author_facet Armbrust, Lee
Bilyk, Alex
Brown, Christopher L.
Healy, Peter C.
author_sort Armbrust, Lee
collection PubMed
description The title compound, C(18)H(20)N(2)O(2), has been synthesized by the reaction of terephthaloyl chloride and 1,2,3,6-tetra­hydro­pyridine. This compound crystallizes as discrete mol­ecular species disposed about a crystallographic centre of symmetry, such that half the mol­ecule constitutes the asymmetric unit. The structure shows an envelope conformation for the dehydro­piperidine ring with the amide carbonyl twisted out of the benzene ring plane by 57.3 (2)°.
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spelling pubmed-29149912010-12-30 1,4-Bis(piperidin-1-ylcarbon­yl)benzene Armbrust, Lee Bilyk, Alex Brown, Christopher L. Healy, Peter C. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(18)H(20)N(2)O(2), has been synthesized by the reaction of terephthaloyl chloride and 1,2,3,6-tetra­hydro­pyridine. This compound crystallizes as discrete mol­ecular species disposed about a crystallographic centre of symmetry, such that half the mol­ecule constitutes the asymmetric unit. The structure shows an envelope conformation for the dehydro­piperidine ring with the amide carbonyl twisted out of the benzene ring plane by 57.3 (2)°. International Union of Crystallography 2007-12-06 /pmc/articles/PMC2914991/ /pubmed/21200873 http://dx.doi.org/10.1107/S1600536807062423 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Armbrust, Lee
Bilyk, Alex
Brown, Christopher L.
Healy, Peter C.
1,4-Bis(piperidin-1-ylcarbon­yl)benzene
title 1,4-Bis(piperidin-1-ylcarbon­yl)benzene
title_full 1,4-Bis(piperidin-1-ylcarbon­yl)benzene
title_fullStr 1,4-Bis(piperidin-1-ylcarbon­yl)benzene
title_full_unstemmed 1,4-Bis(piperidin-1-ylcarbon­yl)benzene
title_short 1,4-Bis(piperidin-1-ylcarbon­yl)benzene
title_sort 1,4-bis(piperidin-1-ylcarbon­yl)benzene
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2914991/
https://www.ncbi.nlm.nih.gov/pubmed/21200873
http://dx.doi.org/10.1107/S1600536807062423
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AT brownchristopherl 14bispiperidin1ylcarbonylbenzene
AT healypeterc 14bispiperidin1ylcarbonylbenzene

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