Doxofyllinium tetra­chloridoanti­monate(III) monohydrate

The title compound, (C(11)H(14)N(4)O(4))[SbCl(4)]·H(2)O, comprises a protonated doxofyllinium cation [7-(1,3-dioxolan-2-ylmeth­yl)-1,3-dimethyl-2,6-dioxo-3,7-dihydro-1H-purin-9-ium], an [SbCl(4)](−) anion and a water mol­ecule linked by N—H⋯O and O—H⋯Cl hydrogen bonds: the [SbCl(4)](−) anions form c...

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Autores principales: Wei, Wan Xing, Feng, Wen-Jie, Zheng, Bo-Jiöng, Chen, Ying, Jin, Zhi-Min
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Metal-Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915103/
https://www.ncbi.nlm.nih.gov/pubmed/21200515
http://dx.doi.org/10.1107/S1600536807065774
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author Wei, Wan Xing
Feng, Wen-Jie
Zheng, Bo-Jiöng
Chen, Ying
Jin, Zhi-Min
author_facet Wei, Wan Xing
Feng, Wen-Jie
Zheng, Bo-Jiöng
Chen, Ying
Jin, Zhi-Min
author_sort Wei, Wan Xing
collection PubMed
description The title compound, (C(11)H(14)N(4)O(4))[SbCl(4)]·H(2)O, comprises a protonated doxofyllinium cation [7-(1,3-dioxolan-2-ylmeth­yl)-1,3-dimethyl-2,6-dioxo-3,7-dihydro-1H-purin-9-ium], an [SbCl(4)](−) anion and a water mol­ecule linked by N—H⋯O and O—H⋯Cl hydrogen bonds: the [SbCl(4)](−) anions form centrosymmetric dimers via weak Sb⋯Cl inter­actions [Sb⋯Cl = 3.1159 (9) Å]. The geometrical arrangement in the crystal structure is characterized by slipped π–π stacking of the parallel purine ring systems, with an inter­planar separation of 3.32 Å.
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spelling pubmed-29151032010-12-30 Doxofyllinium tetra­chloridoanti­monate(III) monohydrate Wei, Wan Xing Feng, Wen-Jie Zheng, Bo-Jiöng Chen, Ying Jin, Zhi-Min Acta Crystallogr Sect E Struct Rep Online Metal-Organic Papers The title compound, (C(11)H(14)N(4)O(4))[SbCl(4)]·H(2)O, comprises a protonated doxofyllinium cation [7-(1,3-dioxolan-2-ylmeth­yl)-1,3-dimethyl-2,6-dioxo-3,7-dihydro-1H-purin-9-ium], an [SbCl(4)](−) anion and a water mol­ecule linked by N—H⋯O and O—H⋯Cl hydrogen bonds: the [SbCl(4)](−) anions form centrosymmetric dimers via weak Sb⋯Cl inter­actions [Sb⋯Cl = 3.1159 (9) Å]. The geometrical arrangement in the crystal structure is characterized by slipped π–π stacking of the parallel purine ring systems, with an inter­planar separation of 3.32 Å. International Union of Crystallography 2007-12-12 /pmc/articles/PMC2915103/ /pubmed/21200515 http://dx.doi.org/10.1107/S1600536807065774 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Metal-Organic Papers
Wei, Wan Xing
Feng, Wen-Jie
Zheng, Bo-Jiöng
Chen, Ying
Jin, Zhi-Min
Doxofyllinium tetra­chloridoanti­monate(III) monohydrate
title Doxofyllinium tetra­chloridoanti­monate(III) monohydrate
title_full Doxofyllinium tetra­chloridoanti­monate(III) monohydrate
title_fullStr Doxofyllinium tetra­chloridoanti­monate(III) monohydrate
title_full_unstemmed Doxofyllinium tetra­chloridoanti­monate(III) monohydrate
title_short Doxofyllinium tetra­chloridoanti­monate(III) monohydrate
title_sort doxofyllinium tetra­chloridoanti­monate(iii) monohydrate
topic Metal-Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915103/
https://www.ncbi.nlm.nih.gov/pubmed/21200515
http://dx.doi.org/10.1107/S1600536807065774
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