3α,6α-Bis(ethoxy­carbon­yl)glycoluril (diethyl 2,5-dioxoperhydro­imidazo[4,5-d]imidazole-3a,6a-dicarboxyl­ate)

The title compound, C(10)H(14)N(4)O(6), crystallizes with two independent mol­ecules in the asymmetric unit. An extensive network of N—H⋯O and C—H⋯O inter­molecular hydrogen bonds stabilizes the crystal packing. One ethyl group is disordered over two positions; the site occupancy factors are 0.68 an...

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Detalles Bibliográficos
Autores principales: Wang, Yu-Zhou, Wang, Zhi-Guo, Li, Lin
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915195/
https://www.ncbi.nlm.nih.gov/pubmed/21200689
http://dx.doi.org/10.1107/S1600536807056292
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author Wang, Yu-Zhou
Wang, Zhi-Guo
Li, Lin
author_facet Wang, Yu-Zhou
Wang, Zhi-Guo
Li, Lin
author_sort Wang, Yu-Zhou
collection PubMed
description The title compound, C(10)H(14)N(4)O(6), crystallizes with two independent mol­ecules in the asymmetric unit. An extensive network of N—H⋯O and C—H⋯O inter­molecular hydrogen bonds stabilizes the crystal packing. One ethyl group is disordered over two positions; the site occupancy factors are 0.68 and 0.32.
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spelling pubmed-29151952010-12-30 3α,6α-Bis(ethoxy­carbon­yl)glycoluril (diethyl 2,5-dioxoperhydro­imidazo[4,5-d]imidazole-3a,6a-dicarboxyl­ate) Wang, Yu-Zhou Wang, Zhi-Guo Li, Lin Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(10)H(14)N(4)O(6), crystallizes with two independent mol­ecules in the asymmetric unit. An extensive network of N—H⋯O and C—H⋯O inter­molecular hydrogen bonds stabilizes the crystal packing. One ethyl group is disordered over two positions; the site occupancy factors are 0.68 and 0.32. International Union of Crystallography 2007-12-06 /pmc/articles/PMC2915195/ /pubmed/21200689 http://dx.doi.org/10.1107/S1600536807056292 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Wang, Yu-Zhou
Wang, Zhi-Guo
Li, Lin
3α,6α-Bis(ethoxy­carbon­yl)glycoluril (diethyl 2,5-dioxoperhydro­imidazo[4,5-d]imidazole-3a,6a-dicarboxyl­ate)
title 3α,6α-Bis(ethoxy­carbon­yl)glycoluril (diethyl 2,5-dioxoperhydro­imidazo[4,5-d]imidazole-3a,6a-dicarboxyl­ate)
title_full 3α,6α-Bis(ethoxy­carbon­yl)glycoluril (diethyl 2,5-dioxoperhydro­imidazo[4,5-d]imidazole-3a,6a-dicarboxyl­ate)
title_fullStr 3α,6α-Bis(ethoxy­carbon­yl)glycoluril (diethyl 2,5-dioxoperhydro­imidazo[4,5-d]imidazole-3a,6a-dicarboxyl­ate)
title_full_unstemmed 3α,6α-Bis(ethoxy­carbon­yl)glycoluril (diethyl 2,5-dioxoperhydro­imidazo[4,5-d]imidazole-3a,6a-dicarboxyl­ate)
title_short 3α,6α-Bis(ethoxy­carbon­yl)glycoluril (diethyl 2,5-dioxoperhydro­imidazo[4,5-d]imidazole-3a,6a-dicarboxyl­ate)
title_sort 3α,6α-bis(ethoxy­carbon­yl)glycoluril (diethyl 2,5-dioxoperhydro­imidazo[4,5-d]imidazole-3a,6a-dicarboxyl­ate)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915195/
https://www.ncbi.nlm.nih.gov/pubmed/21200689
http://dx.doi.org/10.1107/S1600536807056292
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