1,3,5-Tris(2H-tetra­zol-5-ylmeth­oxy)­benzene

The title compound, C(12)H(12)N(12)O(3), was obtained by the hydro­thermal reaction of 1,3,5-tricyano­methoxy­benzene and (CH(3))(3)SiN(3). The mol­ecule is almost planar, with an r.m.s. deviation of 0.0976 Å from the plane through all atoms in the mol­ecule. The three tetra­zole rings make dihedral...

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Detalles Bibliográficos
Autores principales: Luo, Hui-Zhou, Ye, Heng-Yun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915205/
https://www.ncbi.nlm.nih.gov/pubmed/21200700
http://dx.doi.org/10.1107/S1600536807062733
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author Luo, Hui-Zhou
Ye, Heng-Yun
author_facet Luo, Hui-Zhou
Ye, Heng-Yun
author_sort Luo, Hui-Zhou
collection PubMed
description The title compound, C(12)H(12)N(12)O(3), was obtained by the hydro­thermal reaction of 1,3,5-tricyano­methoxy­benzene and (CH(3))(3)SiN(3). The mol­ecule is almost planar, with an r.m.s. deviation of 0.0976 Å from the plane through all atoms in the mol­ecule. The three tetra­zole rings make dihedral angles of 13.09 (19), 2.01 (19) and 11.56 (18)° with one another and corresponding angles of 8.66 (17), 5.44 (16) and 3.51 (17)° with the central benzene ring. In the crystal structure, inter­molecular N—H⋯N hydrogen bonds form well separated one-dimensional planar sheets.
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spelling pubmed-29152052010-12-30 1,3,5-Tris(2H-tetra­zol-5-ylmeth­oxy)­benzene Luo, Hui-Zhou Ye, Heng-Yun Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(12)H(12)N(12)O(3), was obtained by the hydro­thermal reaction of 1,3,5-tricyano­methoxy­benzene and (CH(3))(3)SiN(3). The mol­ecule is almost planar, with an r.m.s. deviation of 0.0976 Å from the plane through all atoms in the mol­ecule. The three tetra­zole rings make dihedral angles of 13.09 (19), 2.01 (19) and 11.56 (18)° with one another and corresponding angles of 8.66 (17), 5.44 (16) and 3.51 (17)° with the central benzene ring. In the crystal structure, inter­molecular N—H⋯N hydrogen bonds form well separated one-dimensional planar sheets. International Union of Crystallography 2007-12-06 /pmc/articles/PMC2915205/ /pubmed/21200700 http://dx.doi.org/10.1107/S1600536807062733 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Luo, Hui-Zhou
Ye, Heng-Yun
1,3,5-Tris(2H-tetra­zol-5-ylmeth­oxy)­benzene
title 1,3,5-Tris(2H-tetra­zol-5-ylmeth­oxy)­benzene
title_full 1,3,5-Tris(2H-tetra­zol-5-ylmeth­oxy)­benzene
title_fullStr 1,3,5-Tris(2H-tetra­zol-5-ylmeth­oxy)­benzene
title_full_unstemmed 1,3,5-Tris(2H-tetra­zol-5-ylmeth­oxy)­benzene
title_short 1,3,5-Tris(2H-tetra­zol-5-ylmeth­oxy)­benzene
title_sort 1,3,5-tris(2h-tetra­zol-5-ylmeth­oxy)­benzene
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915205/
https://www.ncbi.nlm.nih.gov/pubmed/21200700
http://dx.doi.org/10.1107/S1600536807062733
work_keys_str_mv AT luohuizhou 135tris2htetrazol5ylmethoxybenzene
AT yehengyun 135tris2htetrazol5ylmethoxybenzene

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