1-(2-Nitro­phen­yl)-3-phenyl­thio­urea

The title compound, C(13)H(11)N(3)O(2)S, was prepared by reaction of 2-nitro­benzenamine, KOH and 1-isothio­cyanato­benzene in an ethanol solution at room temperature. The dihedral angles formed between the thiourea plane and the phenyl rings are 61.9 and 31.0°. The dihedral angle between the two ph...

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Detalles Bibliográficos
Autores principales: Qin, Yongqi, Jian, Fangfang, Jiang, Mingna, Yang, Xiangyan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915211/
https://www.ncbi.nlm.nih.gov/pubmed/21200707
http://dx.doi.org/10.1107/S1600536807063374
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author Qin, Yongqi
Jian, Fangfang
Jiang, Mingna
Yang, Xiangyan
author_facet Qin, Yongqi
Jian, Fangfang
Jiang, Mingna
Yang, Xiangyan
author_sort Qin, Yongqi
collection PubMed
description The title compound, C(13)H(11)N(3)O(2)S, was prepared by reaction of 2-nitro­benzenamine, KOH and 1-isothio­cyanato­benzene in an ethanol solution at room temperature. The dihedral angles formed between the thiourea plane and the phenyl rings are 61.9 and 31.0°. The dihedral angle between the two phenyl rings is 78.1°. In the crystal structure, there are weak inter­molecular N—H⋯S and C—H⋯S hydrogen-bonding inter­actions.
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spelling pubmed-29152112010-12-30 1-(2-Nitro­phen­yl)-3-phenyl­thio­urea Qin, Yongqi Jian, Fangfang Jiang, Mingna Yang, Xiangyan Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(13)H(11)N(3)O(2)S, was prepared by reaction of 2-nitro­benzenamine, KOH and 1-isothio­cyanato­benzene in an ethanol solution at room temperature. The dihedral angles formed between the thiourea plane and the phenyl rings are 61.9 and 31.0°. The dihedral angle between the two phenyl rings is 78.1°. In the crystal structure, there are weak inter­molecular N—H⋯S and C—H⋯S hydrogen-bonding inter­actions. International Union of Crystallography 2007-12-06 /pmc/articles/PMC2915211/ /pubmed/21200707 http://dx.doi.org/10.1107/S1600536807063374 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Qin, Yongqi
Jian, Fangfang
Jiang, Mingna
Yang, Xiangyan
1-(2-Nitro­phen­yl)-3-phenyl­thio­urea
title 1-(2-Nitro­phen­yl)-3-phenyl­thio­urea
title_full 1-(2-Nitro­phen­yl)-3-phenyl­thio­urea
title_fullStr 1-(2-Nitro­phen­yl)-3-phenyl­thio­urea
title_full_unstemmed 1-(2-Nitro­phen­yl)-3-phenyl­thio­urea
title_short 1-(2-Nitro­phen­yl)-3-phenyl­thio­urea
title_sort 1-(2-nitro­phen­yl)-3-phenyl­thio­urea
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915211/
https://www.ncbi.nlm.nih.gov/pubmed/21200707
http://dx.doi.org/10.1107/S1600536807063374
work_keys_str_mv AT qinyongqi 12nitrophenyl3phenylthiourea
AT jianfangfang 12nitrophenyl3phenylthiourea
AT jiangmingna 12nitrophenyl3phenylthiourea
AT yangxiangyan 12nitrophenyl3phenylthiourea

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