4-(4-Chloro­phen­yl)-5-(4-nitro­phen­yl)-3-phenyl-4H-1,2,4-triazole

The title compound, C(20)H(13)ClN(4)O(2), was synthesized by the condensation of 4-nitro­benzohydrazide and N-(4-chlorophen­yl)­benzimidoyl chloride in N,N-dimethyl­acetamide. The asymmetric unit contains two independent mol­ecules. In one molecule, the triazole ring is oriented at dihedral angles o...

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Detalles Bibliográficos
Autores principales: Hu, Jing, Song, Hongguang, Chen, Guofeng, Ma, Guochun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915251/
https://www.ncbi.nlm.nih.gov/pubmed/21200752
http://dx.doi.org/10.1107/S1600536807063854
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author Hu, Jing
Song, Hongguang
Chen, Guofeng
Ma, Guochun
author_facet Hu, Jing
Song, Hongguang
Chen, Guofeng
Ma, Guochun
author_sort Hu, Jing
collection PubMed
description The title compound, C(20)H(13)ClN(4)O(2), was synthesized by the condensation of 4-nitro­benzohydrazide and N-(4-chlorophen­yl)­benzimidoyl chloride in N,N-dimethyl­acetamide. The asymmetric unit contains two independent mol­ecules. In one molecule, the triazole ring is oriented at dihedral angles of 23.1 (5), 85.4 (1) and 10.5 (1)° with respect to the phenyl, chlorophenyl and nitrophenyl rings, respectively. In the other molecule, the corresponding dihedral angles are 29.8 (9), 73.4 (7) and 16.4 (3)°.
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spelling pubmed-29152512010-12-30 4-(4-Chloro­phen­yl)-5-(4-nitro­phen­yl)-3-phenyl-4H-1,2,4-triazole Hu, Jing Song, Hongguang Chen, Guofeng Ma, Guochun Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(20)H(13)ClN(4)O(2), was synthesized by the condensation of 4-nitro­benzohydrazide and N-(4-chlorophen­yl)­benzimidoyl chloride in N,N-dimethyl­acetamide. The asymmetric unit contains two independent mol­ecules. In one molecule, the triazole ring is oriented at dihedral angles of 23.1 (5), 85.4 (1) and 10.5 (1)° with respect to the phenyl, chlorophenyl and nitrophenyl rings, respectively. In the other molecule, the corresponding dihedral angles are 29.8 (9), 73.4 (7) and 16.4 (3)°. International Union of Crystallography 2007-12-06 /pmc/articles/PMC2915251/ /pubmed/21200752 http://dx.doi.org/10.1107/S1600536807063854 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Hu, Jing
Song, Hongguang
Chen, Guofeng
Ma, Guochun
4-(4-Chloro­phen­yl)-5-(4-nitro­phen­yl)-3-phenyl-4H-1,2,4-triazole
title 4-(4-Chloro­phen­yl)-5-(4-nitro­phen­yl)-3-phenyl-4H-1,2,4-triazole
title_full 4-(4-Chloro­phen­yl)-5-(4-nitro­phen­yl)-3-phenyl-4H-1,2,4-triazole
title_fullStr 4-(4-Chloro­phen­yl)-5-(4-nitro­phen­yl)-3-phenyl-4H-1,2,4-triazole
title_full_unstemmed 4-(4-Chloro­phen­yl)-5-(4-nitro­phen­yl)-3-phenyl-4H-1,2,4-triazole
title_short 4-(4-Chloro­phen­yl)-5-(4-nitro­phen­yl)-3-phenyl-4H-1,2,4-triazole
title_sort 4-(4-chloro­phen­yl)-5-(4-nitro­phen­yl)-3-phenyl-4h-1,2,4-triazole
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915251/
https://www.ncbi.nlm.nih.gov/pubmed/21200752
http://dx.doi.org/10.1107/S1600536807063854
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AT chenguofeng 44chlorophenyl54nitrophenyl3phenyl4h124triazole
AT maguochun 44chlorophenyl54nitrophenyl3phenyl4h124triazole

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