Cinchonidinium chloride monohydrate

In the title salt, C(19)H(23)N(2)O(+)·Cl(−)·H(2)O, the ions and the water mol­ecule are held together by O—H⋯Cl, N—H⋯Cl, O—H⋯O, O—H⋯N and C—H⋯Cl hydrogen bonds, forming a three-dimensional framework. The vinyl group is disordered over two orientations with refined occupancies of 0.564 (16) and 0.436...

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Detalles Bibliográficos
Autores principales: Ni, Shi-Feng, Ma, Lin Lin, Zhao, Gui Fang, Sun, Wen Ji, Jin, Zhi Min
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915256/
https://www.ncbi.nlm.nih.gov/pubmed/21200758
http://dx.doi.org/10.1107/S160053680706343X
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author Ni, Shi-Feng
Ma, Lin Lin
Zhao, Gui Fang
Sun, Wen Ji
Jin, Zhi Min
author_facet Ni, Shi-Feng
Ma, Lin Lin
Zhao, Gui Fang
Sun, Wen Ji
Jin, Zhi Min
author_sort Ni, Shi-Feng
collection PubMed
description In the title salt, C(19)H(23)N(2)O(+)·Cl(−)·H(2)O, the ions and the water mol­ecule are held together by O—H⋯Cl, N—H⋯Cl, O—H⋯O, O—H⋯N and C—H⋯Cl hydrogen bonds, forming a three-dimensional framework. The vinyl group is disordered over two orientations with refined occupancies of 0.564 (16) and 0.436 (16). The cell parameters of the title compound have been reported previously [Griffiths (1952 ▶). Acta Cryst. 5, 290–291].
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spelling pubmed-29152562010-12-30 Cinchonidinium chloride monohydrate Ni, Shi-Feng Ma, Lin Lin Zhao, Gui Fang Sun, Wen Ji Jin, Zhi Min Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title salt, C(19)H(23)N(2)O(+)·Cl(−)·H(2)O, the ions and the water mol­ecule are held together by O—H⋯Cl, N—H⋯Cl, O—H⋯O, O—H⋯N and C—H⋯Cl hydrogen bonds, forming a three-dimensional framework. The vinyl group is disordered over two orientations with refined occupancies of 0.564 (16) and 0.436 (16). The cell parameters of the title compound have been reported previously [Griffiths (1952 ▶). Acta Cryst. 5, 290–291]. International Union of Crystallography 2007-12-06 /pmc/articles/PMC2915256/ /pubmed/21200758 http://dx.doi.org/10.1107/S160053680706343X Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Ni, Shi-Feng
Ma, Lin Lin
Zhao, Gui Fang
Sun, Wen Ji
Jin, Zhi Min
Cinchonidinium chloride monohydrate
title Cinchonidinium chloride monohydrate
title_full Cinchonidinium chloride monohydrate
title_fullStr Cinchonidinium chloride monohydrate
title_full_unstemmed Cinchonidinium chloride monohydrate
title_short Cinchonidinium chloride monohydrate
title_sort cinchonidinium chloride monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915256/
https://www.ncbi.nlm.nih.gov/pubmed/21200758
http://dx.doi.org/10.1107/S160053680706343X
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AT malinlin cinchonidiniumchloridemonohydrate
AT zhaoguifang cinchonidiniumchloridemonohydrate
AT sunwenji cinchonidiniumchloridemonohydrate
AT jinzhimin cinchonidiniumchloridemonohydrate

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