3,4-Dihydr­oxy-N′-(2-hydroxy­benzyl­idene)benzohydrazide–methanol–water (2/1/3)

The asymmetric unit of the title compound, C(14)H(12)N(2)O(4)·0.5CH(4)O·1.5H(2)O, consists of two Schiff base mol­ecules, three water mol­ecules and one methanol mol­ecule. The dihedral angle between the two benzene rings is 7.8 (2)° in one of the mol­ecules and 4.0 (2)° in the other. Intra­molecula...

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Detalles Bibliográficos
Autores principales: Ma, Hong-Bo, Huang, Shan-Shan, Diao, Yun-Peng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915271/
https://www.ncbi.nlm.nih.gov/pubmed/21200776
http://dx.doi.org/10.1107/S1600536807065038
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author Ma, Hong-Bo
Huang, Shan-Shan
Diao, Yun-Peng
author_facet Ma, Hong-Bo
Huang, Shan-Shan
Diao, Yun-Peng
author_sort Ma, Hong-Bo
collection PubMed
description The asymmetric unit of the title compound, C(14)H(12)N(2)O(4)·0.5CH(4)O·1.5H(2)O, consists of two Schiff base mol­ecules, three water mol­ecules and one methanol mol­ecule. The dihedral angle between the two benzene rings is 7.8 (2)° in one of the mol­ecules and 4.0 (2)° in the other. Intra­molecular O—H⋯O and O—H⋯N hydrogen bonds are observed. Mol­ecules are linked into a three-dimensional network by O—H⋯O and N—H⋯O inter­molecular hydrogen bonds.
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spelling pubmed-29152712010-12-30 3,4-Dihydr­oxy-N′-(2-hydroxy­benzyl­idene)benzohydrazide–methanol–water (2/1/3) Ma, Hong-Bo Huang, Shan-Shan Diao, Yun-Peng Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(14)H(12)N(2)O(4)·0.5CH(4)O·1.5H(2)O, consists of two Schiff base mol­ecules, three water mol­ecules and one methanol mol­ecule. The dihedral angle between the two benzene rings is 7.8 (2)° in one of the mol­ecules and 4.0 (2)° in the other. Intra­molecular O—H⋯O and O—H⋯N hydrogen bonds are observed. Mol­ecules are linked into a three-dimensional network by O—H⋯O and N—H⋯O inter­molecular hydrogen bonds. International Union of Crystallography 2007-12-06 /pmc/articles/PMC2915271/ /pubmed/21200776 http://dx.doi.org/10.1107/S1600536807065038 Text en © Ma et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ma, Hong-Bo
Huang, Shan-Shan
Diao, Yun-Peng
3,4-Dihydr­oxy-N′-(2-hydroxy­benzyl­idene)benzohydrazide–methanol–water (2/1/3)
title 3,4-Dihydr­oxy-N′-(2-hydroxy­benzyl­idene)benzohydrazide–methanol–water (2/1/3)
title_full 3,4-Dihydr­oxy-N′-(2-hydroxy­benzyl­idene)benzohydrazide–methanol–water (2/1/3)
title_fullStr 3,4-Dihydr­oxy-N′-(2-hydroxy­benzyl­idene)benzohydrazide–methanol–water (2/1/3)
title_full_unstemmed 3,4-Dihydr­oxy-N′-(2-hydroxy­benzyl­idene)benzohydrazide–methanol–water (2/1/3)
title_short 3,4-Dihydr­oxy-N′-(2-hydroxy­benzyl­idene)benzohydrazide–methanol–water (2/1/3)
title_sort 3,4-dihydr­oxy-n′-(2-hydroxy­benzyl­idene)benzohydrazide–methanol–water (2/1/3)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915271/
https://www.ncbi.nlm.nih.gov/pubmed/21200776
http://dx.doi.org/10.1107/S1600536807065038
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