7-[4-(5,7-Dimethyl-1,8-naphthyridin-2-yl­oxy)phen­oxy]-2,4-dimethyl-1,8-naphthyridine methanol disolvate

The title compound, C(26)H(22)N(4)O(2)·2CH(3)OH, was synthesized and characterized by (1)H NMR spectroscopy and X-ray structure analysis. There is one half-mol­ecule in the asymmetric unit with a centre of symmetry located at the centre of the benzene ring. The two bridged naphthyridine ring systems...

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Detalles Bibliográficos
Autores principales: Jin, Shou-Wen, Wang, Da-Qi, Chen, Yun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915306/
https://www.ncbi.nlm.nih.gov/pubmed/21200814
http://dx.doi.org/10.1107/S160053680706549X
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author Jin, Shou-Wen
Wang, Da-Qi
Chen, Yun
author_facet Jin, Shou-Wen
Wang, Da-Qi
Chen, Yun
author_sort Jin, Shou-Wen
collection PubMed
description The title compound, C(26)H(22)N(4)O(2)·2CH(3)OH, was synthesized and characterized by (1)H NMR spectroscopy and X-ray structure analysis. There is one half-mol­ecule in the asymmetric unit with a centre of symmetry located at the centre of the benzene ring. The two bridged naphthyridine ring systems are in an anti­parallel orientation. In the crystal structure, O—H⋯N, C—H⋯O and C—H⋯N inter­actions define the packing.
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spelling pubmed-29153062010-12-30 7-[4-(5,7-Dimethyl-1,8-naphthyridin-2-yl­oxy)phen­oxy]-2,4-dimethyl-1,8-naphthyridine methanol disolvate Jin, Shou-Wen Wang, Da-Qi Chen, Yun Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(26)H(22)N(4)O(2)·2CH(3)OH, was synthesized and characterized by (1)H NMR spectroscopy and X-ray structure analysis. There is one half-mol­ecule in the asymmetric unit with a centre of symmetry located at the centre of the benzene ring. The two bridged naphthyridine ring systems are in an anti­parallel orientation. In the crystal structure, O—H⋯N, C—H⋯O and C—H⋯N inter­actions define the packing. International Union of Crystallography 2007-12-12 /pmc/articles/PMC2915306/ /pubmed/21200814 http://dx.doi.org/10.1107/S160053680706549X Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Jin, Shou-Wen
Wang, Da-Qi
Chen, Yun
7-[4-(5,7-Dimethyl-1,8-naphthyridin-2-yl­oxy)phen­oxy]-2,4-dimethyl-1,8-naphthyridine methanol disolvate
title 7-[4-(5,7-Dimethyl-1,8-naphthyridin-2-yl­oxy)phen­oxy]-2,4-dimethyl-1,8-naphthyridine methanol disolvate
title_full 7-[4-(5,7-Dimethyl-1,8-naphthyridin-2-yl­oxy)phen­oxy]-2,4-dimethyl-1,8-naphthyridine methanol disolvate
title_fullStr 7-[4-(5,7-Dimethyl-1,8-naphthyridin-2-yl­oxy)phen­oxy]-2,4-dimethyl-1,8-naphthyridine methanol disolvate
title_full_unstemmed 7-[4-(5,7-Dimethyl-1,8-naphthyridin-2-yl­oxy)phen­oxy]-2,4-dimethyl-1,8-naphthyridine methanol disolvate
title_short 7-[4-(5,7-Dimethyl-1,8-naphthyridin-2-yl­oxy)phen­oxy]-2,4-dimethyl-1,8-naphthyridine methanol disolvate
title_sort 7-[4-(5,7-dimethyl-1,8-naphthyridin-2-yl­oxy)phen­oxy]-2,4-dimethyl-1,8-naphthyridine methanol disolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915306/
https://www.ncbi.nlm.nih.gov/pubmed/21200814
http://dx.doi.org/10.1107/S160053680706549X
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AT chenyun 7457dimethyl18naphthyridin2yloxyphenoxy24dimethyl18naphthyridinemethanoldisolvate

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