1,1′-Binaphthalene-2,2′-diyl hydrogen phosphate

The title compound, racemic bnppa, C(20)H(13)O(4)P, crystallizes with four mol­ecules in the asymmetric unit. Two independent centrosymmetric O—H⋯O hydrogen-bonded tetra­mers, each involving two of the symmetry-independent mol­ecules in the asymmetric unit generate the packing motif in the crystal s...

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Detalles Bibliográficos
Autores principales: Nayak, Susanta K., Chandrasekhar, S., Row, T. N. Guru
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915313/
https://www.ncbi.nlm.nih.gov/pubmed/21200821
http://dx.doi.org/10.1107/S1600536807064343
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author Nayak, Susanta K.
Chandrasekhar, S.
Row, T. N. Guru
author_facet Nayak, Susanta K.
Chandrasekhar, S.
Row, T. N. Guru
author_sort Nayak, Susanta K.
collection PubMed
description The title compound, racemic bnppa, C(20)H(13)O(4)P, crystallizes with four mol­ecules in the asymmetric unit. Two independent centrosymmetric O—H⋯O hydrogen-bonded tetra­mers, each involving two of the symmetry-independent mol­ecules in the asymmetric unit generate the packing motif in the crystal structure. The hydro­phobic parts of the tetra­mers connect to their neighbours via C—H⋯π and π–π inter­actions [3.899 (2), 3.895 (2) and 3.803 (2) Å within the symmetric unit, 3.851 (2), 4.000 (2), 3.988 (2) and 3.905 (2) Å across centres of symmetry].
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spelling pubmed-29153132010-12-30 1,1′-Binaphthalene-2,2′-diyl hydrogen phosphate Nayak, Susanta K. Chandrasekhar, S. Row, T. N. Guru Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, racemic bnppa, C(20)H(13)O(4)P, crystallizes with four mol­ecules in the asymmetric unit. Two independent centrosymmetric O—H⋯O hydrogen-bonded tetra­mers, each involving two of the symmetry-independent mol­ecules in the asymmetric unit generate the packing motif in the crystal structure. The hydro­phobic parts of the tetra­mers connect to their neighbours via C—H⋯π and π–π inter­actions [3.899 (2), 3.895 (2) and 3.803 (2) Å within the symmetric unit, 3.851 (2), 4.000 (2), 3.988 (2) and 3.905 (2) Å across centres of symmetry]. International Union of Crystallography 2007-12-12 /pmc/articles/PMC2915313/ /pubmed/21200821 http://dx.doi.org/10.1107/S1600536807064343 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Nayak, Susanta K.
Chandrasekhar, S.
Row, T. N. Guru
1,1′-Binaphthalene-2,2′-diyl hydrogen phosphate
title 1,1′-Binaphthalene-2,2′-diyl hydrogen phosphate
title_full 1,1′-Binaphthalene-2,2′-diyl hydrogen phosphate
title_fullStr 1,1′-Binaphthalene-2,2′-diyl hydrogen phosphate
title_full_unstemmed 1,1′-Binaphthalene-2,2′-diyl hydrogen phosphate
title_short 1,1′-Binaphthalene-2,2′-diyl hydrogen phosphate
title_sort 1,1′-binaphthalene-2,2′-diyl hydrogen phosphate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915313/
https://www.ncbi.nlm.nih.gov/pubmed/21200821
http://dx.doi.org/10.1107/S1600536807064343
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AT chandrasekhars 11binaphthalene22diylhydrogenphosphate
AT rowtnguru 11binaphthalene22diylhydrogenphosphate

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