7-(1,3-Dioxolan-2-ylmeth­yl)-1,3-di­methyl­purine-2,6(1H,3H)-dione trichloro­acetic acid solvate

In the title compound, C(11)H(14)N(4)O(4)·C(2)HCl(3)O(2), the dioxolane ring adopts an envelope conformation. Doxophylline [7-(1,3-dioxolan-2-yl-meth­yl)-1,3-dimethyl-3,7-dihydro-1H-purine-2,6-dione] and trichloro­acetic acid mol­ecules are linked by O—H⋯N and C—H⋯O hydrogen bonds.

Detalles Bibliográficos
Autores principales: Wu, Xiang-Xiang, Shu, Zhan, Ma, Lin-Lin, Ding, Zhe-Wu, Jin, Zhi-Min
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2007
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915388/
https://www.ncbi.nlm.nih.gov/pubmed/21200909
http://dx.doi.org/10.1107/S1600536807067025
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author Wu, Xiang-Xiang
Shu, Zhan
Ma, Lin-Lin
Ding, Zhe-Wu
Jin, Zhi-Min
author_facet Wu, Xiang-Xiang
Shu, Zhan
Ma, Lin-Lin
Ding, Zhe-Wu
Jin, Zhi-Min
author_sort Wu, Xiang-Xiang
collection PubMed
description In the title compound, C(11)H(14)N(4)O(4)·C(2)HCl(3)O(2), the dioxolane ring adopts an envelope conformation. Doxophylline [7-(1,3-dioxolan-2-yl-meth­yl)-1,3-dimethyl-3,7-dihydro-1H-purine-2,6-dione] and trichloro­acetic acid mol­ecules are linked by O—H⋯N and C—H⋯O hydrogen bonds.
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spelling pubmed-29153882010-12-30 7-(1,3-Dioxolan-2-ylmeth­yl)-1,3-di­methyl­purine-2,6(1H,3H)-dione trichloro­acetic acid solvate Wu, Xiang-Xiang Shu, Zhan Ma, Lin-Lin Ding, Zhe-Wu Jin, Zhi-Min Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(11)H(14)N(4)O(4)·C(2)HCl(3)O(2), the dioxolane ring adopts an envelope conformation. Doxophylline [7-(1,3-dioxolan-2-yl-meth­yl)-1,3-dimethyl-3,7-dihydro-1H-purine-2,6-dione] and trichloro­acetic acid mol­ecules are linked by O—H⋯N and C—H⋯O hydrogen bonds. International Union of Crystallography 2007-12-21 /pmc/articles/PMC2915388/ /pubmed/21200909 http://dx.doi.org/10.1107/S1600536807067025 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Wu, Xiang-Xiang
Shu, Zhan
Ma, Lin-Lin
Ding, Zhe-Wu
Jin, Zhi-Min
7-(1,3-Dioxolan-2-ylmeth­yl)-1,3-di­methyl­purine-2,6(1H,3H)-dione trichloro­acetic acid solvate
title 7-(1,3-Dioxolan-2-ylmeth­yl)-1,3-di­methyl­purine-2,6(1H,3H)-dione trichloro­acetic acid solvate
title_full 7-(1,3-Dioxolan-2-ylmeth­yl)-1,3-di­methyl­purine-2,6(1H,3H)-dione trichloro­acetic acid solvate
title_fullStr 7-(1,3-Dioxolan-2-ylmeth­yl)-1,3-di­methyl­purine-2,6(1H,3H)-dione trichloro­acetic acid solvate
title_full_unstemmed 7-(1,3-Dioxolan-2-ylmeth­yl)-1,3-di­methyl­purine-2,6(1H,3H)-dione trichloro­acetic acid solvate
title_short 7-(1,3-Dioxolan-2-ylmeth­yl)-1,3-di­methyl­purine-2,6(1H,3H)-dione trichloro­acetic acid solvate
title_sort 7-(1,3-dioxolan-2-ylmeth­yl)-1,3-di­methyl­purine-2,6(1h,3h)-dione trichloro­acetic acid solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2915388/
https://www.ncbi.nlm.nih.gov/pubmed/21200909
http://dx.doi.org/10.1107/S1600536807067025
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