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N′-[4-(Dimethyl­amino)­benzyl­idene]-4-meth­oxybenzohydrazide

The title Schiff base compound, C(17)H(19)N(3)O(2), was obtained from the condensation of 4-dimethyl­amino­benzaldehyde with 4-methoxy­benzohydrazide in an ethanol solution. The mol­ecule is twisted with respect to the N—N single bond [C—N—N—C = −159.27 (14)°] and the dihedral angle between the two...

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Autor principal: Lu, Jiu-Fu
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959335/
https://www.ncbi.nlm.nih.gov/pubmed/21201227
http://dx.doi.org/10.1107/S1600536808031012
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author Lu, Jiu-Fu
author_facet Lu, Jiu-Fu
author_sort Lu, Jiu-Fu
collection PubMed
description The title Schiff base compound, C(17)H(19)N(3)O(2), was obtained from the condensation of 4-dimethyl­amino­benzaldehyde with 4-methoxy­benzohydrazide in an ethanol solution. The mol­ecule is twisted with respect to the N—N single bond [C—N—N—C = −159.27 (14)°] and the dihedral angle between the two aromatic rings is 67.1 (2)°. In the crystal structure, the mol­ecules are linked into chains along the c axis by inter­molecular N—H⋯O and C—H⋯O hydrogen bonds.
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spelling pubmed-29593352010-12-30 N′-[4-(Dimethyl­amino)­benzyl­idene]-4-meth­oxybenzohydrazide Lu, Jiu-Fu Acta Crystallogr Sect E Struct Rep Online Organic Papers The title Schiff base compound, C(17)H(19)N(3)O(2), was obtained from the condensation of 4-dimethyl­amino­benzaldehyde with 4-methoxy­benzohydrazide in an ethanol solution. The mol­ecule is twisted with respect to the N—N single bond [C—N—N—C = −159.27 (14)°] and the dihedral angle between the two aromatic rings is 67.1 (2)°. In the crystal structure, the mol­ecules are linked into chains along the c axis by inter­molecular N—H⋯O and C—H⋯O hydrogen bonds. International Union of Crystallography 2008-09-30 /pmc/articles/PMC2959335/ /pubmed/21201227 http://dx.doi.org/10.1107/S1600536808031012 Text en © Jiu-Fu Lu 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Lu, Jiu-Fu
N′-[4-(Dimethyl­amino)­benzyl­idene]-4-meth­oxybenzohydrazide
title N′-[4-(Dimethyl­amino)­benzyl­idene]-4-meth­oxybenzohydrazide
title_full N′-[4-(Dimethyl­amino)­benzyl­idene]-4-meth­oxybenzohydrazide
title_fullStr N′-[4-(Dimethyl­amino)­benzyl­idene]-4-meth­oxybenzohydrazide
title_full_unstemmed N′-[4-(Dimethyl­amino)­benzyl­idene]-4-meth­oxybenzohydrazide
title_short N′-[4-(Dimethyl­amino)­benzyl­idene]-4-meth­oxybenzohydrazide
title_sort n′-[4-(dimethyl­amino)­benzyl­idene]-4-meth­oxybenzohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959335/
https://www.ncbi.nlm.nih.gov/pubmed/21201227
http://dx.doi.org/10.1107/S1600536808031012
work_keys_str_mv AT lujiufu n4dimethylaminobenzylidene4methoxybenzohydrazide