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4-Hydr­oxy-N′-(2-hydr­oxy-3-methoxy­benzyl­idene)benzohydrazide mono­hydrate

In the title compound, C(15)H(14)N(2)O(4)·H(2)O, the dihedral angle between the two aromatic rings is 33.3 (5)°. The meth­oxy group is twisted slightly away from the attached benzene ring [C—O—C—C = 13.8 (9)°]. An intra­molecular O—H⋯N hydrogen bond is observed. In the crystal structure, the mol­ecu...

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Detalles Bibliográficos
Autor principal: Lu, Jiu-Fu
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959387/
https://www.ncbi.nlm.nih.gov/pubmed/21201226
http://dx.doi.org/10.1107/S1600536808030894
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author Lu, Jiu-Fu
author_facet Lu, Jiu-Fu
author_sort Lu, Jiu-Fu
collection PubMed
description In the title compound, C(15)H(14)N(2)O(4)·H(2)O, the dihedral angle between the two aromatic rings is 33.3 (5)°. The meth­oxy group is twisted slightly away from the attached benzene ring [C—O—C—C = 13.8 (9)°]. An intra­molecular O—H⋯N hydrogen bond is observed. In the crystal structure, the mol­ecules are linked into a two-dimensional network parallel to the (010) plane by inter­molecular N—H⋯O, O—H⋯O and C—H⋯O hydrogen bonds
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spelling pubmed-29593872010-12-30 4-Hydr­oxy-N′-(2-hydr­oxy-3-methoxy­benzyl­idene)benzohydrazide mono­hydrate Lu, Jiu-Fu Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(14)N(2)O(4)·H(2)O, the dihedral angle between the two aromatic rings is 33.3 (5)°. The meth­oxy group is twisted slightly away from the attached benzene ring [C—O—C—C = 13.8 (9)°]. An intra­molecular O—H⋯N hydrogen bond is observed. In the crystal structure, the mol­ecules are linked into a two-dimensional network parallel to the (010) plane by inter­molecular N—H⋯O, O—H⋯O and C—H⋯O hydrogen bonds International Union of Crystallography 2008-09-27 /pmc/articles/PMC2959387/ /pubmed/21201226 http://dx.doi.org/10.1107/S1600536808030894 Text en © Jiu-Fu Lu 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Lu, Jiu-Fu
4-Hydr­oxy-N′-(2-hydr­oxy-3-methoxy­benzyl­idene)benzohydrazide mono­hydrate
title 4-Hydr­oxy-N′-(2-hydr­oxy-3-methoxy­benzyl­idene)benzohydrazide mono­hydrate
title_full 4-Hydr­oxy-N′-(2-hydr­oxy-3-methoxy­benzyl­idene)benzohydrazide mono­hydrate
title_fullStr 4-Hydr­oxy-N′-(2-hydr­oxy-3-methoxy­benzyl­idene)benzohydrazide mono­hydrate
title_full_unstemmed 4-Hydr­oxy-N′-(2-hydr­oxy-3-methoxy­benzyl­idene)benzohydrazide mono­hydrate
title_short 4-Hydr­oxy-N′-(2-hydr­oxy-3-methoxy­benzyl­idene)benzohydrazide mono­hydrate
title_sort 4-hydr­oxy-n′-(2-hydr­oxy-3-methoxy­benzyl­idene)benzohydrazide mono­hydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959387/
https://www.ncbi.nlm.nih.gov/pubmed/21201226
http://dx.doi.org/10.1107/S1600536808030894
work_keys_str_mv AT lujiufu 4hydroxyn2hydroxy3methoxybenzylidenebenzohydrazidemonohydrate