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4-Hydroxy-N′-(2-hydroxy-3-methoxybenzylidene)benzohydrazide monohydrate
In the title compound, C(15)H(14)N(2)O(4)·H(2)O, the dihedral angle between the two aromatic rings is 33.3 (5)°. The methoxy group is twisted slightly away from the attached benzene ring [C—O—C—C = 13.8 (9)°]. An intramolecular O—H⋯N hydrogen bond is observed. In the crystal structure, the molecu...
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2008
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Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959387/ https://www.ncbi.nlm.nih.gov/pubmed/21201226 http://dx.doi.org/10.1107/S1600536808030894 |
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author | Lu, Jiu-Fu |
author_facet | Lu, Jiu-Fu |
author_sort | Lu, Jiu-Fu |
collection | PubMed |
description | In the title compound, C(15)H(14)N(2)O(4)·H(2)O, the dihedral angle between the two aromatic rings is 33.3 (5)°. The methoxy group is twisted slightly away from the attached benzene ring [C—O—C—C = 13.8 (9)°]. An intramolecular O—H⋯N hydrogen bond is observed. In the crystal structure, the molecules are linked into a two-dimensional network parallel to the (010) plane by intermolecular N—H⋯O, O—H⋯O and C—H⋯O hydrogen bonds |
format | Text |
id | pubmed-2959387 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2008 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29593872010-12-30 4-Hydroxy-N′-(2-hydroxy-3-methoxybenzylidene)benzohydrazide monohydrate Lu, Jiu-Fu Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(14)N(2)O(4)·H(2)O, the dihedral angle between the two aromatic rings is 33.3 (5)°. The methoxy group is twisted slightly away from the attached benzene ring [C—O—C—C = 13.8 (9)°]. An intramolecular O—H⋯N hydrogen bond is observed. In the crystal structure, the molecules are linked into a two-dimensional network parallel to the (010) plane by intermolecular N—H⋯O, O—H⋯O and C—H⋯O hydrogen bonds International Union of Crystallography 2008-09-27 /pmc/articles/PMC2959387/ /pubmed/21201226 http://dx.doi.org/10.1107/S1600536808030894 Text en © Jiu-Fu Lu 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Lu, Jiu-Fu 4-Hydroxy-N′-(2-hydroxy-3-methoxybenzylidene)benzohydrazide monohydrate |
title | 4-Hydroxy-N′-(2-hydroxy-3-methoxybenzylidene)benzohydrazide monohydrate |
title_full | 4-Hydroxy-N′-(2-hydroxy-3-methoxybenzylidene)benzohydrazide monohydrate |
title_fullStr | 4-Hydroxy-N′-(2-hydroxy-3-methoxybenzylidene)benzohydrazide monohydrate |
title_full_unstemmed | 4-Hydroxy-N′-(2-hydroxy-3-methoxybenzylidene)benzohydrazide monohydrate |
title_short | 4-Hydroxy-N′-(2-hydroxy-3-methoxybenzylidene)benzohydrazide monohydrate |
title_sort | 4-hydroxy-n′-(2-hydroxy-3-methoxybenzylidene)benzohydrazide monohydrate |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959387/ https://www.ncbi.nlm.nih.gov/pubmed/21201226 http://dx.doi.org/10.1107/S1600536808030894 |
work_keys_str_mv | AT lujiufu 4hydroxyn2hydroxy3methoxybenzylidenebenzohydrazidemonohydrate |