(2R)-N-[5-(4-Chloro­phen­yl)-1,3,4-thia­diazol-2-yl]-2-(cinnamoylamino)propanamide

In the title compound, C(20)H(17)ClN(4)O(2)S, the dihedral angle between the two benzene rings is 65.9 (1)°; the corresponding angle between the 4-chloro­phenyl and thia­diazole rings is 3.4 (8)°. The conformations of the N—H and C=O bonds are anti with respect to each other. The enone groups show a...

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Autores principales: Li, Shao-Hua, Huang, Hui-Ming, Kuang, Bin-Hai, Tu, Guo-Gang, Liu, Cheng-Mei
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959416/
https://www.ncbi.nlm.nih.gov/pubmed/21201204
http://dx.doi.org/10.1107/S1600536808030353
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author Li, Shao-Hua
Huang, Hui-Ming
Kuang, Bin-Hai
Tu, Guo-Gang
Liu, Cheng-Mei
author_facet Li, Shao-Hua
Huang, Hui-Ming
Kuang, Bin-Hai
Tu, Guo-Gang
Liu, Cheng-Mei
author_sort Li, Shao-Hua
collection PubMed
description In the title compound, C(20)H(17)ClN(4)O(2)S, the dihedral angle between the two benzene rings is 65.9 (1)°; the corresponding angle between the 4-chloro­phenyl and thia­diazole rings is 3.4 (8)°. The conformations of the N—H and C=O bonds are anti with respect to each other. The enone groups show a trans configuration. The structure displays intermolecular N—H⋯O, C—H⋯N, C—H⋯S and C—H⋯O hydrogen bonding.
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spelling pubmed-29594162010-12-30 (2R)-N-[5-(4-Chloro­phen­yl)-1,3,4-thia­diazol-2-yl]-2-(cinnamoylamino)propanamide Li, Shao-Hua Huang, Hui-Ming Kuang, Bin-Hai Tu, Guo-Gang Liu, Cheng-Mei Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(20)H(17)ClN(4)O(2)S, the dihedral angle between the two benzene rings is 65.9 (1)°; the corresponding angle between the 4-chloro­phenyl and thia­diazole rings is 3.4 (8)°. The conformations of the N—H and C=O bonds are anti with respect to each other. The enone groups show a trans configuration. The structure displays intermolecular N—H⋯O, C—H⋯N, C—H⋯S and C—H⋯O hydrogen bonding. International Union of Crystallography 2008-09-24 /pmc/articles/PMC2959416/ /pubmed/21201204 http://dx.doi.org/10.1107/S1600536808030353 Text en © Li et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Shao-Hua
Huang, Hui-Ming
Kuang, Bin-Hai
Tu, Guo-Gang
Liu, Cheng-Mei
(2R)-N-[5-(4-Chloro­phen­yl)-1,3,4-thia­diazol-2-yl]-2-(cinnamoylamino)propanamide
title (2R)-N-[5-(4-Chloro­phen­yl)-1,3,4-thia­diazol-2-yl]-2-(cinnamoylamino)propanamide
title_full (2R)-N-[5-(4-Chloro­phen­yl)-1,3,4-thia­diazol-2-yl]-2-(cinnamoylamino)propanamide
title_fullStr (2R)-N-[5-(4-Chloro­phen­yl)-1,3,4-thia­diazol-2-yl]-2-(cinnamoylamino)propanamide
title_full_unstemmed (2R)-N-[5-(4-Chloro­phen­yl)-1,3,4-thia­diazol-2-yl]-2-(cinnamoylamino)propanamide
title_short (2R)-N-[5-(4-Chloro­phen­yl)-1,3,4-thia­diazol-2-yl]-2-(cinnamoylamino)propanamide
title_sort (2r)-n-[5-(4-chloro­phen­yl)-1,3,4-thia­diazol-2-yl]-2-(cinnamoylamino)propanamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959416/
https://www.ncbi.nlm.nih.gov/pubmed/21201204
http://dx.doi.org/10.1107/S1600536808030353
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