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5-Methyl-1-(3-nitro­benz­yl)-1H-1,2,3-triazole-4-carboxylic acid monohydrate

The title compound, C(11)H(10)N(4)O(4)·H(2)O, was synthesized from 1-azido­methyl-3-nitro­benzene and ethyl acetyl­acetate. Single-crystal X-ray analysis reveals that the dihedral angle between the triazole and benzene ring planes is 84.80 (2)°. The packing of the mol­ecules is stabilized by strong...

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Detalles Bibliográficos
Autores principales: Xiao, Jie, Wang, Wen Xiang, Zhao, Hong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959515/
https://www.ncbi.nlm.nih.gov/pubmed/21580950
http://dx.doi.org/10.1107/S1600536808030584
Descripción
Sumario:The title compound, C(11)H(10)N(4)O(4)·H(2)O, was synthesized from 1-azido­methyl-3-nitro­benzene and ethyl acetyl­acetate. Single-crystal X-ray analysis reveals that the dihedral angle between the triazole and benzene ring planes is 84.80 (2)°. The packing of the mol­ecules is stabilized by strong O—H⋯O hydrogen bonds involving the solvent water mol­ecules as donors and acceptors. The resulting layers are arranged into a three-dimensional framework via weak C—H⋯O inter­actions.