tert-Butyl N-benzyl-N-[4-(4-fluoro­benzoyl­meth­yl)-2-pyrid­yl]carbamate

In the crystal structure of the title compound, C(25)H(25)FN(2)O(3), the pyridine ring makes dihedral angles of 75.1 (3), 39.4 (3) and 74.6 (3)° with the phenyl ring, the carbamate plane and the 4-fluoro­phenyl ring, respectively. The phenyl ring makes dihedral angles of 77.2 (3) and 23.6 (3)° with...

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Detalles Bibliográficos
Autores principales: Koch, Pierre, Schollmeyer, Dieter, Laufer, Stefan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959675/
https://www.ncbi.nlm.nih.gov/pubmed/21581076
http://dx.doi.org/10.1107/S160053680803448X
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author Koch, Pierre
Schollmeyer, Dieter
Laufer, Stefan
author_facet Koch, Pierre
Schollmeyer, Dieter
Laufer, Stefan
author_sort Koch, Pierre
collection PubMed
description In the crystal structure of the title compound, C(25)H(25)FN(2)O(3), the pyridine ring makes dihedral angles of 75.1 (3), 39.4 (3) and 74.6 (3)° with the phenyl ring, the carbamate plane and the 4-fluoro­phenyl ring, respectively. The phenyl ring makes dihedral angles of 77.2 (3) and 23.6 (3)° with the carbamate plane and the 4-fluoro­phenyl ring, respectively. The 4-fluoro­phenyl ring is perpendicular to the carbamate plane, the dihedral angle between them being 89.5 (3)°.
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spelling pubmed-29596752010-12-30 tert-Butyl N-benzyl-N-[4-(4-fluoro­benzoyl­meth­yl)-2-pyrid­yl]carbamate Koch, Pierre Schollmeyer, Dieter Laufer, Stefan Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title compound, C(25)H(25)FN(2)O(3), the pyridine ring makes dihedral angles of 75.1 (3), 39.4 (3) and 74.6 (3)° with the phenyl ring, the carbamate plane and the 4-fluoro­phenyl ring, respectively. The phenyl ring makes dihedral angles of 77.2 (3) and 23.6 (3)° with the carbamate plane and the 4-fluoro­phenyl ring, respectively. The 4-fluoro­phenyl ring is perpendicular to the carbamate plane, the dihedral angle between them being 89.5 (3)°. International Union of Crystallography 2008-10-31 /pmc/articles/PMC2959675/ /pubmed/21581076 http://dx.doi.org/10.1107/S160053680803448X Text en © Koch et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Koch, Pierre
Schollmeyer, Dieter
Laufer, Stefan
tert-Butyl N-benzyl-N-[4-(4-fluoro­benzoyl­meth­yl)-2-pyrid­yl]carbamate
title tert-Butyl N-benzyl-N-[4-(4-fluoro­benzoyl­meth­yl)-2-pyrid­yl]carbamate
title_full tert-Butyl N-benzyl-N-[4-(4-fluoro­benzoyl­meth­yl)-2-pyrid­yl]carbamate
title_fullStr tert-Butyl N-benzyl-N-[4-(4-fluoro­benzoyl­meth­yl)-2-pyrid­yl]carbamate
title_full_unstemmed tert-Butyl N-benzyl-N-[4-(4-fluoro­benzoyl­meth­yl)-2-pyrid­yl]carbamate
title_short tert-Butyl N-benzyl-N-[4-(4-fluoro­benzoyl­meth­yl)-2-pyrid­yl]carbamate
title_sort tert-butyl n-benzyl-n-[4-(4-fluoro­benzoyl­meth­yl)-2-pyrid­yl]carbamate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959675/
https://www.ncbi.nlm.nih.gov/pubmed/21581076
http://dx.doi.org/10.1107/S160053680803448X
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AT schollmeyerdieter tertbutylnbenzyln44fluorobenzoylmethyl2pyridylcarbamate
AT lauferstefan tertbutylnbenzyln44fluorobenzoylmethyl2pyridylcarbamate

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