(E)-3-Bromo-N′-(5-bromo-2-hydroxy­benzyl­idene)benzohydrazide

The title compound, C(14)H(10)Br(2)N(2)O(2), was synthesized by the reaction of 5-bromo­salicylaldehyde with an equimolar quantity of 3-bromo­benzohydrazide in methanol. The dihedral angle between the two benzene rings is 10.5 (4)°. In the crystal structure, mol­ecules are linked through inter­molec...

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Detalles Bibliográficos
Autores principales: Qu, Lan-Zhu, Yang, Tao, Cao, Guo-Biao, Wang, Xiao-Ya
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959678/
https://www.ncbi.nlm.nih.gov/pubmed/21580927
http://dx.doi.org/10.1107/S1600536808030675
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author Qu, Lan-Zhu
Yang, Tao
Cao, Guo-Biao
Wang, Xiao-Ya
author_facet Qu, Lan-Zhu
Yang, Tao
Cao, Guo-Biao
Wang, Xiao-Ya
author_sort Qu, Lan-Zhu
collection PubMed
description The title compound, C(14)H(10)Br(2)N(2)O(2), was synthesized by the reaction of 5-bromo­salicylaldehyde with an equimolar quantity of 3-bromo­benzohydrazide in methanol. The dihedral angle between the two benzene rings is 10.5 (4)°. In the crystal structure, mol­ecules are linked through inter­molecular N—H⋯O hydrogen bonds to form chains parallel to the c axis, and an intra­molecular O—H⋯N inter­action also occurs.
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spelling pubmed-29596782010-12-30 (E)-3-Bromo-N′-(5-bromo-2-hydroxy­benzyl­idene)benzohydrazide Qu, Lan-Zhu Yang, Tao Cao, Guo-Biao Wang, Xiao-Ya Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(10)Br(2)N(2)O(2), was synthesized by the reaction of 5-bromo­salicylaldehyde with an equimolar quantity of 3-bromo­benzohydrazide in methanol. The dihedral angle between the two benzene rings is 10.5 (4)°. In the crystal structure, mol­ecules are linked through inter­molecular N—H⋯O hydrogen bonds to form chains parallel to the c axis, and an intra­molecular O—H⋯N inter­action also occurs. International Union of Crystallography 2008-10-04 /pmc/articles/PMC2959678/ /pubmed/21580927 http://dx.doi.org/10.1107/S1600536808030675 Text en © Qu et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Qu, Lan-Zhu
Yang, Tao
Cao, Guo-Biao
Wang, Xiao-Ya
(E)-3-Bromo-N′-(5-bromo-2-hydroxy­benzyl­idene)benzohydrazide
title (E)-3-Bromo-N′-(5-bromo-2-hydroxy­benzyl­idene)benzohydrazide
title_full (E)-3-Bromo-N′-(5-bromo-2-hydroxy­benzyl­idene)benzohydrazide
title_fullStr (E)-3-Bromo-N′-(5-bromo-2-hydroxy­benzyl­idene)benzohydrazide
title_full_unstemmed (E)-3-Bromo-N′-(5-bromo-2-hydroxy­benzyl­idene)benzohydrazide
title_short (E)-3-Bromo-N′-(5-bromo-2-hydroxy­benzyl­idene)benzohydrazide
title_sort (e)-3-bromo-n′-(5-bromo-2-hydroxy­benzyl­idene)benzohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959678/
https://www.ncbi.nlm.nih.gov/pubmed/21580927
http://dx.doi.org/10.1107/S1600536808030675
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