(E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N-(2-naphth­yl)cyclo­propane­carboxamide

The title compound, C(19)H(17)ClF(3)NO, was synthesized from 3-[(E)-2-chloro-3,3,3-trifluoro­prop-1-en­yl]-2,2-dimethyl­cyclopropane­carboxylic acid and 2-aminona­phthalene. There are two molecules in the asymmetric unit. The dihedral angle between the naphthalene and cyclo­propane units is 111.6 (5...

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Detalles Bibliográficos
Autores principales: Liu, Dong-Qing, Yan, Fan-Yong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959779/
https://www.ncbi.nlm.nih.gov/pubmed/21581049
http://dx.doi.org/10.1107/S1600536808032078
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author Liu, Dong-Qing
Yan, Fan-Yong
author_facet Liu, Dong-Qing
Yan, Fan-Yong
author_sort Liu, Dong-Qing
collection PubMed
description The title compound, C(19)H(17)ClF(3)NO, was synthesized from 3-[(E)-2-chloro-3,3,3-trifluoro­prop-1-en­yl]-2,2-dimethyl­cyclopropane­carboxylic acid and 2-aminona­phthalene. There are two molecules in the asymmetric unit. The dihedral angle between the naphthalene and cyclo­propane units is 111.6 (5)°. Molecules are connected into chains by intermol­ecular N—H⋯O hydrogen bonds. One of the Cl atoms is disordered over two positions with occupancies 0.653 (15) and 0.347 (15).
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spelling pubmed-29597792010-12-30 (E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N-(2-naphth­yl)cyclo­propane­carboxamide Liu, Dong-Qing Yan, Fan-Yong Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(19)H(17)ClF(3)NO, was synthesized from 3-[(E)-2-chloro-3,3,3-trifluoro­prop-1-en­yl]-2,2-dimethyl­cyclopropane­carboxylic acid and 2-aminona­phthalene. There are two molecules in the asymmetric unit. The dihedral angle between the naphthalene and cyclo­propane units is 111.6 (5)°. Molecules are connected into chains by intermol­ecular N—H⋯O hydrogen bonds. One of the Cl atoms is disordered over two positions with occupancies 0.653 (15) and 0.347 (15). International Union of Crystallography 2008-10-25 /pmc/articles/PMC2959779/ /pubmed/21581049 http://dx.doi.org/10.1107/S1600536808032078 Text en © Liu and Yan 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Liu, Dong-Qing
Yan, Fan-Yong
(E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N-(2-naphth­yl)cyclo­propane­carboxamide
title (E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N-(2-naphth­yl)cyclo­propane­carboxamide
title_full (E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N-(2-naphth­yl)cyclo­propane­carboxamide
title_fullStr (E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N-(2-naphth­yl)cyclo­propane­carboxamide
title_full_unstemmed (E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N-(2-naphth­yl)cyclo­propane­carboxamide
title_short (E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N-(2-naphth­yl)cyclo­propane­carboxamide
title_sort (e)-3-(2-chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-n-(2-naphth­yl)cyclo­propane­carboxamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959779/
https://www.ncbi.nlm.nih.gov/pubmed/21581049
http://dx.doi.org/10.1107/S1600536808032078
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AT yanfanyong e32chloro333trifluoroprop1enyl22dimethyln2naphthylcyclopropanecarboxamide

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